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Nucleation, growth, and superlattice formation of nanocrystals observed in liquid cell transmission electron microscopy

Published online by Cambridge University Press:  10 September 2020

Qian Chen ,
Jong Min Yuk ,
Matthew R. Hauwiller ,
Jungjae Park ,
Kyun Seong Dae ,
Jae Sung Kim  and
A. Paul Alivisatos
Qian Chen
Affiliation:
Department of Materials Science and Engineering, University of Illinois at Urbana-Champaign, USA; qchen20@illinois.edu
Jong Min Yuk
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Korea; jongmin.yuk@kaist.ac.kr
Matthew R. Hauwiller
Affiliation:
Department of Materials Science and Engineering, Massachusetts Institute of Technology, USA; mhauwill@mit.edu
Jungjae Park
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Korea; jungjae10@kaist.ac.kr
Kyun Seong Dae
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Korea; ddalgi1051@kaist.ac.kr
Jae Sung Kim
Affiliation:
Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology, Korea; ijs7596@kaist.ac.kr
A. Paul Alivisatos
Affiliation:
University of California, Berkeley; Kavli Energy Nanoscience Institute; Lawrence Berkeley National Laboratory, USA; paul.alivisatos@berkeley.edu
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Abstract

This article reviews the advancements and prospects of liquid cell transmission electron microscopy (TEM) imaging and analysis methods in understanding the nucleation, growth, etching, and assembly dynamics of nanocrystals. The bonding of atoms into nanoscale crystallites produces materials with nonadditive properties unique to their size and geometry. The recent application of in situ liquid cell TEM to nanocrystal development has initiated a paradigm shift, (1) from trial-and-error synthesis to a mechanistic understanding of the “synthetic reactions” responsible for the emergence of crystallites from a disordered soup of reactive species (e.g., ions, atoms, molecules) and shape-defined growth or etching; and (2) from post-processing characterization of the nanocrystals’ superlattice assemblies to in situ imaging and mapping of the fundamental interactions and energy landscape governing their collective phase behaviors. Imaging nanocrystal formation and assembly processes on the single-particle level in solution immediately impacts many existing fields, including materials science, nanochemistry, colloidal science, biology, environmental science, electrochemistry, mineralization, soft condensed-matter physics, and device fabrication.

Type
Liquid Phase Electron Microscopy
Information
MRS Bulletin , Volume 45 , Issue 9: Liquid Phase Electron Microscopy , September 2020 , pp. 713 - 726
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Copyright
Copyright © Materials Research Society 2020

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