Hostname: page-component-8448b6f56d-jr42d Total loading time: 0 Render date: 2024-04-24T00:44:13.041Z Has data issue: false hasContentIssue false

Resolving an Anomolous Radiocarbon Determination on Mastodon Bone from Monte Verde, Chile

Published online by Cambridge University Press:  20 January 2017

Debra George
Affiliation:
Molecular Anthropology Laboratory, Department of Anthropology, University of California, Davis, CA95616
John Southon
Affiliation:
Keck Carbon Cycle Accelerator Mass Spectrometry Laboratory, Department of Earth System Science, University of California, Irvine, CA 92697-3100
R. E. Taylor
Affiliation:
Department of Anthropology, University of California, Riverside, CA 92521; Cotsen Institute of Archaeology, University of California, Los Angeles, CA 90024; Keck Carbon Cycle Accelerator Mass Spectrometry Laboratory, Department of Earth System Science, University of California, Irvine, CA 92697-3100

Abstract

Previous 14C determinations obtained on two segments of a single mastodon bone recovered from Monte Verde, Chile, were highly discordant, differing by more than 5,000 years. Because of the significance of this site in discussions concerning the earliest peopling of the Western Hemisphere, additional 14C and new δ13C values have been obtained on organic fractions isolated from both segments. The constituent amino acid profiles indicate that both bone segments retain significant amounts of protein (mostly collagen) residues. Four accelerator mass spectrometry-based 14C values obtained on total amino acids and ultrafiltered gelatin fractions—two from each segment—are statistically identical and indicate an age of 12,460 (± 30) BP for the mastodon. This value is concordant with 14C values obtained on other culturally affiliated organics associated with the MV-II levels at this site.

Résumé

Résumé

Anteriormente, las determinaciones 14C obtenidas de dos segmentos de un solo hueso de mastodonte recolectado del depósito arqueológico en Monte Verde, Chile, no correspondían, registrando una diferencia de mas de 5,000 años. Debido a la importancia de este sitio en el diálogo sobre el poblamiento del nuevo mundo, han sido analizadas muestras adicionales de los mismos segmentos de hueso. Los valores de 14C y δ13 son derivados de fracciones orgánicas aislados de ambos segmentos. Los perfiles de aminoácidos indican que ambos segmentos guardaron cantidades significativos de proteína (la mayoría en forma de colágeno) residual. Cuatro valores 14C (AMS) obtenidos de las dos fracciones aminoácidos total y gelatina ultrafiltrada—dos de cada segmento—son idénticos, según las estadísticas, e indican una edad de 12,460(± 30) años AP (antes presente) para el mastodonte. Este valor es consistente con los valores de 14C obtenidos en otros materiales orgánicos culturalmente asociados con las capas MV-II del sitio.

Type
Reports
Copyright
Copyright © The Society for American Archaeology 2005

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

References Cited

Adovasio, James M., and Pedler, David R. 1997 Monte Verde and the Antiquity of Humankind in the Americas. Antiquity 71: 573580.Google Scholar
Ajie, Henry O., Kaplan, Ian R., Hauschka, Peter V., Kirner, Donna L., Slota, Peter J. Jr. Taylor, R. E., 1992 Radiocarbon Dating of Bone Osteocalcin: Isolating and Characterizing a Non-Collagen Protein. Radiocarbon 34: 296305.Google Scholar
Ajie, Henry O., Kaplan, Ian R., Slota, Peter J. Jr., and Taylor, R. E. 1990 AMS Radiocarbon Dating of Bone Osteocalcin. Nuclear Instruments and Methods in Physics Research B52: 433437.CrossRefGoogle Scholar
Brown, Thomas A., Nelson, D. Earle, Vogel, John, and Southon, John 1988 Improved Collagen Extraction by Modified Longin Method. Radiocarbon 30: 171177.CrossRefGoogle Scholar
Burky, Richard R. 1996 Radiocarbon Dating Archaeologically Significant Bone Using Gamma-Carboxyglutamic Acid (Gla) and Alpha-Carboxyglycine (Aminomalonate). Unpublished Ph.D. dissertation, University of California, Riverside.Google Scholar
Burky, Richard R., Kirner, Donna L., Taylor, R. E., Hare, P. Edgar, and Southon, John 1998 14C Dating of Bone Using γ-Carboxyglutamic Acid and α-Carboxyglycine (Aminomalonate). Radiocarbon 40: 1120.Google Scholar
Collins, Michael B. 1999 Reply to Fiedel, Part II. Discovering Archaeology [Special Report] 1(6): 1415.Google Scholar
Dickinson, William R. 2004 Migration Pathways. Geotimes 49(5): 6.Google Scholar
Dillehay, Tom D. 1989 Monte Verde: A Late Pleistocene Settlement in Chile, Vol. I: Paleoenvironment and Site Context. Smithsonian Institution Press, Washington, D.C. Google Scholar
Dillehay, Tom D. 1997a Monte Verde: A Late Pleistocene Settlement in Chile, Vol. 2: The Archaeological Context and Interpretation. Smithsonian Institution Press, Washington, D.C. Google Scholar
Dillehay, Tom D. 1997 b Site Findings: Activity Pattering of the Archaeological Remains. In Monte Verde: A Late Pleistocene Settlement in Chile, Vol. 2: The Archeological Context and Interpretation, by Dillehay, Tom D., pp. 767788. Smithsonian Institution Press, Washington, D.C. Google Scholar
Dillehay, Tom D., and Collins, Michael B. 1991 Monte Verde, Chile: A Comment on Lynch. American Antiquity 56: 333341.Google Scholar
Dillehay, Tom D., and Pino, Mario 1989 Stratigraphy and Chronology. In Monte Verde: A Late Pleistocene Settlement in Chile, Vol. I: Paleoenvironment and Site Context, by Dillehay, Tom D., pp. 133145. Smithsonian Institution Press, Washington, D.C. Google Scholar
Dillehay, Tom D., and Pino, Mario 1997a Radiocarbon Chronology. In Monte Verde: A Late Pleistocene Settlement in Chile, Vol. 2: The Archeological Context and Interpretation, by Dillehay, Tom D., pp. 4152. Smithsonian Institution Press, Washington, D.C. Google Scholar
Dillehay, Tom D., and Pino, Mario 1997b Site Setting and Strategy. In Monte Verde: A Late Pleistocene Settlement in Chile, Vol. 2: The Archeological Context and Interpretation, by Dillehay, Tom D., pp. 2540. Smithsonian Institution Press, Washington, D.C. Google Scholar
Dillehay, Tom D., Pino, D., Rossen, J., Ocampo, C., Rivas, P. L., Pollack, D., 1999 Reply to Fiedel, Part I. Discovering Archaeology [Special Report] 1(6): 12–14.Google Scholar
Fiedel, Stewart J. 1999 Artifact provenience at Monte Verde: Confusion and Contradictions. Discovering Archaeology [Special Report], 1(6): 1–12.Google Scholar
Haynes C., Vance, Jr. 1999 Monte Verde and the Pre-Clovis Situation in America. Discovering Archaeology/Scientific American (special report) 1(6): 1719.Google Scholar
Hedges, Robert E. M., and Klinken, G. J. van 1992 A Review of Current Approaches in the Pretreatment of Bone for Radiocarbon Dating by AMS. Radiocarbon 34(3): 279291.Google Scholar
Law, Ian A., and Hedges, Robert E. M. 1989 A Semi-Automated Bone Pretreatment System and the Pretreatment of Older and Contaminated Samples. Radiocarbon 31: 247253.CrossRefGoogle Scholar
Long, Austin, Wilson, A. T., Ernst, R. D., Gore, B. H., and Hare, P. Edgar 1989 AMS Radiocarbon Dating of Bones at Arizona. Radiocarbon 31: 231238.Google Scholar
Lynch, Thomas F. 1990 Glacial-Age Man in South America? A Critical Review. American Antiquity 55: 1236.Google Scholar
Lynch, Thomas F. 1991 Lack of Evidence for Glacial-Age Settlement of South America. American Antiquity 56: 348355.CrossRefGoogle Scholar
Meltzer, David J., Grayson, Donald K., Ardila, G., Barker, A. W., Dincauze, Dena F., Haynes, Vance Jr., Mena, Fernando, Nunez, Laure, and Stanford, Dennis J. 1997 On the Pleistocene Antiquity of Monte Verde, Southern Chile. American Antiquity 62: 659663.Google Scholar
Nagle, C., and Wilcox, U. V. 1982 Monte Verde: Radiocarbon dates from an Early-Man Site in South-Central Chile. Journal of Field Archaeology 9: 547550.Google Scholar
Ramsey, C. B., Higham, T., Bowles, A., and Hedges, Robert 2004 Improvements to the Pretreatment of Bone at Oxford. Radiocarbon 46: 155163.Google Scholar
Schmits, Kamille R. 2004 A Review of Bioarchaeological Thought on the Peopling of the New World. In The Settlement of the American Continents: A Multidisciplinary Approach to Human Biogeography, edited by Michael Barton, C., Colar, Geoffrey A., Yesner, David R., and Pearson, Georges A., pp. 6475. University of Arizona Press, Tucson.Google Scholar
Simkin, Tom, and Sieben, Lee 1994 Volcanoes of the World. 2nd ed. Geoscience Press. Tucson. Analysis of Fossil Bone: Removal of Humâtes with XAD-2 Resin. Geocehmica et Cosmochimica Acta 52: 21972206.Google Scholar
Stafford, Thomas W., Hare, P. Edgar, Currie, L., Jull, A. J. Timothy, and Donahue, Douglas J. 1990 Accuracy of North American Human Skeleton Ages. Quaternary Research 34: 111120.Google Scholar
Stafford, Thomas W., Hare, P. Edgar, Currie, L., Jull, A. J. Timothy, and Donahue, Douglas J. 1987 Study of Bone Radiocarbon Dating Accuracy at the University of Arizona NSF Accelerator Faculty for Radioisotope Analysis. Radiocarbon 29: 2444.Google Scholar
Taylor, R. E. 1987 Radiocarbon Dating: An Archaeological Perspective. Academic Press, New York.Google Scholar
Taylor, R. E. 1992 Radiocarbon Dating of Bone: To Collagen and Beyond. In Radiocarbon after Four Decades: An Interdisciplinary Perspective, edited by Taylor, R. E., Long, Austin, and Kra, Renee, pp. 375–402. Springer Verlag, New York.Google Scholar
Taylor, R. E., Haynes, C. Vance Jr., Kirner, Donna L., and Southon, John 1999 Radiocarbon Analysis of Modem Organics at Monte Verde, Chile: No Evidence for a Local Reservoir Effect. American Antiquity 64: 455460.Google Scholar
Taylor, R. E., Haynes, C. Vance Jr., and Stuiver, Minze 1996 Clovis and Folsom Age Estimates: Stratigraphic Context and Radiocarbon Calibration. Antiquity 70: 515525.Google Scholar
Taylor, R. E., Smith, David Glenn, and Southon, John 2001 The Kennewick Skeleton: Chronological and Biomolecular Contexts. Radiocarbon 43: 965976.Google Scholar
Tuross, Noreen 1997 Organic Preservation at Monte Verde. In Monte Verde: A Late Pleistocene Settlement in Chile, Vol. 2: The Archeological Context and Interpretation, by Dillehay, Thomas D., pp. 7383. Smithsonian Institution Press, Washington. D.C. Google Scholar