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Transmission electron microscopy investigation of tubular and capsular needlelike crystals of C60 produced by the liquid–liquid interfacial precipitation method

  • Kun’ichi Miyazawa (a1) and Tadatomo Suga (a2)
  • DOI: http://dx.doi.org/10.1557/JMR.2004.0409
  • Published online: 01 November 2004
Abstract

Tubular and capsular needlelike crystals of C60 with a few hundreds nanometers to about one micrometer in diameter were discovered among the precipitates prepared by the liquid–liquid interfacial precipitation method. Addition of a small amount of (η2–C60)Pt(PPh3)2 to the toluene solution of C60 produced various morphologies of hollow C60 crystals. This paper gives the first report on the formation of structures we named “C60 nanotubes.”

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a) Address all correspondence to this author. e-mail: miyazawa.kunichi@nims.go.jp
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1K. Miyazawa , Y. Kuwasaki , A. Obayashi and M. Kuwabara : C60 nanowhiskers formed by the liquid-liquid interfacial precipitation method. J. Mater. Res. 17, 83 (2002).

2K. Miyazawa : C70 nanowhiskers fabricated by forming liquid/liquid interfaces in the systems of toluene solution of C70 and isopropyl alcohol. J. Am. Ceram. Soc. 85, 1297 (2002).

3K. Miyazawa , T. Mashino and T. Suga : Structural characterization of the C60[C(COOC2H5)2] whiskers prepared by the liquid–liquid interfacial precipitation method. J. Mater. Res. 18, 2730 (2003).

5M. Tachibana , K. Kobayashi , T. Uchida , K. Kojima , M. Tanimura and K. Miyazawa : Photo-assisted growth and polymerization of C60 ‘nano’whiskers. Chem. Phys. Lett. 374, 279 (2003).

6G. Chambers and H.J. Byrne : Raman spectroscopic study of excited states and photo-polymerisation of C60 from solution. Chem. Phys. Lett. 302, 307 (1999).

7K. Miyazawa and T. Suga : Transmission electron microscopy investigation of fullerene nanowhiskers and needle-like precipitates formed by using C60 and (η2-C60)Pt(PPh3)2. J. Mater. Res. 19, 2410 (2004).

8D. McCready and M. Alnajjar , Powder Diffraction File No. 44-558 (International Centre for Diffraction Data, Newton Square, PA, 1994)

9Y. Iwasa , T. Arima , R.M. Fleming , T. Siegrist , O. Zhou , R.C. Haddon , L.J. Rothberg , K.B. Lyons , H.L. Carter Jr. A.F. Hebard , R. Tycko , G. Dabbagh , J.J. Krajewski , G.A. Thomas and T. Yagi : New phases of C60 Synthesized at high-pressure. Science 264, 1570 (1994).

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Journal of Materials Research
  • ISSN: 0884-2914
  • EISSN: 2044-5326
  • URL: /core/journals/journal-of-materials-research
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