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Characterization of Glue Sizing Layers in Portuguese Wood Paintings from the 15th and 16th Centuries by SEM Secondary Electron Images and μ-FTIR

Published online by Cambridge University Press:  11 October 2013

Vanessa Antunes*
Affiliation:
Instituto de História de Arte–Faculdade de Letras da Universidade de Lisboa (IHA/FLUL), Alameda da Universidade, 1600-214, Lisboa, Portugal
Maria J.Oliveira
Affiliation:
Laboratório José de Figueiredo–Direcção Geral do Património Cultural (LJF/DGPC), R. das Janelas Verdes, 1249-018 Lisboa, Portugal
Helena Vargas
Affiliation:
Laboratório José de Figueiredo–Direcção Geral do Património Cultural (LJF/DGPC), R. das Janelas Verdes, 1249-018 Lisboa, Portugal
António Candeias
Affiliation:
Laboratório José de Figueiredo–Direcção Geral do Património Cultural (LJF/DGPC), R. das Janelas Verdes, 1249-018 Lisboa, Portugal Laboratório HERCULES–Universidade de Évora (UE), Rua Romão Ramalho 59, 7000-676 Évora, Portugal
Ana Seruya
Affiliation:
Centro de Física Atómica–Universidade de Lisboa (CFA/FCUL), Av. Prof. Gama Pinto, 2, 1649-003 Lisboa, Portugal
Luís Dias
Affiliation:
Laboratório HERCULES–Universidade de Évora (UE), Rua Romão Ramalho 59, 7000-676 Évora, Portugal
Vítor Serrão
Affiliation:
Instituto de História de Arte–Faculdade de Letras da Universidade de Lisboa (IHA/FLUL), Alameda da Universidade, 1600-214, Lisboa, Portugal
João Coroado
Affiliation:
Instituto Politécnico de Tomar (IPT), Quinta do Contador, Estrada da Serra, 2300-313 Tomar, Portugal
*
*Corresponding author.vanessahantunes@gmail.com
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Abstract

According to treatises on 15th and 16th century paintings, artists dedicated particular attention to the sizing layer—consisting mainly of animal glue applied onto the wood support before further application of the ground layer. The stability of a painting mainly depends on the presence of a very cohesive sizing layer. However, the study of these layers has not received special attention from researchers. In this article we present a methodology for characterization of the sizing layer both chemically, by IR spectroscopy (Fourier transform infrared spectroscopy), and morphologically, by scanning electron microscopy (SEM). Secondary electron images obtained by SEM allow precise characterization of such layers. Painting reconstructions were used as references in development of the method to study the sizing layer in real painting samples. Presented herein are examples of this study on 15th and 16th century Portuguese paintings, particularly on the Triptych of S. Simão, from the Aveiro Museum, and S. Pedro, belonging to the Mercy of Tavira.

Type
Materials Applications
Copyright
Copyright © Microscopy Society of America 2014 

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References

Anonymous (1794). Segredos necessarios para os officios, Artes, e Manufacturas, e para muitos objectos sobre a economia domestica, extrahidos da Encyclopédia, da Encyclopedia Methodica, da Encyclopedia prática, e das melhores obras que tratarão até agora estes objectos. Lisboa: Officina de Simão Thaddeo Ferreira.Google Scholar
Bruquetas Galán, R. (2002). Técnicas y materiales de la pintura española en los siglos de oro. Madrid: Fundación de Apoyo a la Historia del Arte Hispánico.Google Scholar
Carlyle, L., Boon, J.J., Haswell, R. & Stols-Witlox, M. (2008). Historically accurate ground reconstructions for oil paintings. In Preparation for Paintings : The Artist's Choice and Its Consequences, Townsend, J.H., Doherty, T., Heydenreich, G. & Ridge, J. (Eds.), pp. 110122. London: Archetype Books.Google Scholar
Carlyle, L. & Witlox, M. (2005). Historically accurate reconstructions of artists' oil painting materials. In Art of the Past: Sources and Reconstruction: Proceedings of the First Symposium of the Art Technological Source Research Study Group, Clarke, M., Townsend, J., Stijnman, A. & Instituut Collectie Nederland (Eds.), pp. 5359. London: Archetype Publications with the participation of ICN Amsterdam.Google Scholar
Carlyle, L. & Witlox, M. (2007). Historically accurate reconstructions of artists' oil painting materials. Tate Papers Issue 7, 19 (online journal).Google Scholar
Cennini, C. (1821). Di Cennino Cennini trattato della pittura, Tambroni, G. (Ed.), p. 95. Rome: Salviucci.Google Scholar
Cennini, C., Milanesi, G. & Milanesi, C. (1859). Il libro dell'arte: trattato della pittura di Cennino Cennini, p. 72. Firenze: Felice le Monnier.Google Scholar
Derrick, M.R., Stulik, D. & Landry, J.M. (1999). Infrared Spectroscopy in Conservation Science, Scientific Tools for Conservation. Los Angeles, CA: The Getty Conservation Institute.Google Scholar
Gómez, S.S., Moya, M.S.A. & Rodriguez, A. (2008). Reconstruction of documented preparation methods for gesso grosso and gesso sottile in Spanish School panel paintings. In Art Technology—Sources and Methods, Kroustallis, S., Townsend, J.H., Bruquetas, E.C., Stijnman, A. & Moya, M.S.A. (Eds.), p. 196. London: Archetype Publications.Google Scholar
Gonzalez Lopez, M.J. (1992). Estudio de las preparaciones de pintura sobre soportes de tela y tabla: Caracterizacion de sus principales componentes, comportamiento y factores de deterioro. In Bellas Artes, p. 792. Sevilla: Servicio de Publicaciones de la Universidad de Sevilla.Google Scholar
Hendy, P. & Lucas, A.S. (1968). The ground in pictures. Museum XXI(4), 245276.Google Scholar
Matteini, M. & Moles, A. (1993). La chimica nel restauro: i materiali dell'arte pittorica. Firenze: Nardini.Google Scholar
Monteiro, P. (2006). Apêndice documental. In As matérias da imagem: os pigmentos na tratadística portuguesa entre a Idade Média e 1850, (relatório de projecto), pp. 33, 69. Lisboa: Faculdade de Letras da Universidade de Lisboa.Google Scholar
Monteiro, P. & Afonso, L. (2007). Fontes para o estudo dos pigmentos na tratadística portuguesa: Da Idade Média a 1850. In Artis, revista do Instituto de História da Arte da Faculdade de Letras da Universidade de Lisboa, Barbosa, L.A.G. & Xavier, L.A.G. (Eds.), pp. 161186. Lisboa: Instituto de História da Arte da Faculdade de Letras da Universidade de Lisboa.Google Scholar
Nunes, P. (1982). Arte da Pintura, Symmetria e Perspectiva. In fac-simile da edição de 1615 com um estudo introdutório de Leontina Ventura, 1982, Ventura, L. (Ed.), vol. 101, pp. 125126. Porto: Editorial Paisagem.Google Scholar
Pacheco, F. (2009). Arte de la pintura, Bassegoda i Hugas, Bonaventura (Ed.), p. 782. Madrid: Cátedra.Google Scholar
Santos Gómez, S. (2006). Las preparaciones de yeso en la pintura sobre tabla de la Escuela Española. PhD Thesis, pp. 170–372, Facultad de Bellas Artes. Madrid: Servicio de Publicaciones de Universidad Complutense de Madrid. Google Scholar