Skip to main content

We use cookies to distinguish you from other users and to provide you with a better experience on our websites. Close this message to accept cookies or find out how to manage your cookie settings.

Close cookie message
Cancel
×
×
Home
  • Home
Article
  • Cited by 33
  • Cited by
    Crossref Citations
    Crossref logo
    This article has been cited by the following publications. This list is generated based on data provided by CrossRef.
    Kim, Byung Hyo Yang, Jiwoong Lee, Donghoon Choi, Back Kyu Hyeon, Taeghwan and Park, Jungwon 2018. Liquid-Phase Transmission Electron Microscopy for Studying Colloidal Inorganic Nanoparticles. Advanced Materials, Vol. 30, Issue. 4, p. 1703316.
    Tao, Jinhui Nielsen, Michael H. and De Yoreo, James J. 2018. Nucleation and phase transformation pathways in electrolyte solutions investigated by in situ microscopy techniques. Current Opinion in Colloid & Interface Science, Vol. 34, Issue. , p. 74.
    Kelly, Daniel J. Zhou, Mingwei Clark, Nick Hamer, Matthew J. Lewis, Edward A. Rakowski, Alexander M. Haigh, Sarah J. and Gorbachev, Roman V. 2018. Nanometer Resolution Elemental Mapping in Graphene-Based TEM Liquid Cells. Nano Letters, Vol. 18, Issue. 2, p. 1168.
    Burke, M. G. Bertali, G. Scenini, F. Haigh, S. J. and Prestat, E. 2018. Proceedings of the 18th International Conference on Environmental Degradation of Materials in Nuclear Power Systems – Water Reactors. p. 399.
    Zhang, Shijie Song, Zhengtian Godaliyadda, G. M. Dilshan P. Ye, Dong Hye Chowdhury, Azhad U. Sengupta, Atanu Buzzard, Gregery T. Bouman, Charles A. and Simpson, Garth J. 2018. Dynamic Sparse Sampling for Confocal Raman Microscopy. Analytical Chemistry, Vol. 90, Issue. 7, p. 4461.
    Jinschek, Joerg R. 2017. Achieve atomic resolution in in situ S/TEM experiments to examine complex interface structures in nanomaterials. Current Opinion in Solid State and Materials Science, Vol. 21, Issue. 2, p. 77.
    Dwyer, Jason R. and Harb, Maher 2017. Through a Window, Brightly: A Review of Selected Nanofabricated Thin-Film Platforms for Spectroscopy, Imaging, and Detection. Applied Spectroscopy, Vol. 71, Issue. 9, p. 2051.
    Singh, Sarika Prestat, Eric Huang, Liang-Feng Rondinelli, James M. Haigh, Sarah J. and Rosen, Brian A. 2017. Role of 2D and 3D defects on the reduction of LaNiO3 nanoparticles for catalysis. Scientific Reports, Vol. 7, Issue. 1,
    Yuan, Yifei Amine, Khalil Lu, Jun and Shahbazian-Yassar, Reza 2017. Understanding materials challenges for rechargeable ion batteries with in situ transmission electron microscopy. Nature Communications, Vol. 8, Issue. , p. 15806.
    Ayirala, Subhash C. Al-Enezi, Sultan M. and Al-Yousef, Ali A. 2017. A state of the art review to develop novel workflow for microscopic scale understanding of advanced water flooding mechanisms in carbonates. Journal of Petroleum Science and Engineering, Vol. 157, Issue. , p. 530.
    Schilling, Sibylle Janssen, Arne Zaluzec, Nestor J. and Burke, M. Grace 2017. Practical Aspects of Electrochemical Corrosion Measurements During In Situ Analytical Transmission Electron Microscopy (TEM) of Austenitic Stainless Steel in Aqueous Media. Microscopy and Microanalysis, Vol. 23, Issue. 04, p. 741.
    Prestat, Eric Kulzick, Matthew A. Dietrich, Paul J. Smith, Mr. Matthew Tien, Mr. Eu-Pin Burke, M. Grace Haigh, Sarah J. and Zaluzec, Nestor J. 2017. In Situ Industrial Bimetallic Catalyst Characterization using Scanning Transmission Electron Microscopy and X-ray Absorption Spectroscopy at One Atmosphere and Elevated Temperature. ChemPhysChem, Vol. 18, Issue. 16, p. 2151.
    Luo, Chen Wang, Chaolun Wu, Xing Zhang, Jian and Chu, Junhao 2017. In Situ Transmission Electron Microscopy Characterization and Manipulation of Two-Dimensional Layered Materials beyond Graphene. Small, Vol. 13, Issue. 35, p. 1604259.
    Fraser, Hamish L. Smith, David J. and Wittig, James E. 2017. The scientific careers of Robert Sinclair and Nestor Zaluzec - A brief sketch. Ultramicroscopy, Vol. 176, Issue. , p. 2.
    Burke, M.G. Bertali, G. Prestat, E. Scenini, F. and Haigh, S.J. 2017. The application of in situ analytical transmission electron microscopy to the study of preferential intergranular oxidation in Alloy 600. Ultramicroscopy, Vol. 176, Issue. , p. 46.
    Lewis, Edward A. Downie, Helen Collins, Richard F. Prestat, Eric Lloyd, Jonathan R. and Haigh, Sarah J. 2016. Imaging the Hydrated Microbe-Metal Interface Using Nanoscale Spectrum Imaging. Particle & Particle Systems Characterization, Vol. 33, Issue. 11, p. 833.
    Ross, Frances M. Wang, Chongmin and de Jonge, Niels 2016. Transmission electron microscopy of specimens and processes in liquids. MRS Bulletin, Vol. 41, Issue. 10, p. 791.
    Kelly, D. J. Lewis, E. A. Downie, H. Lloyd, J. R. Zaluzec, N. J. Burke, M. G. and Haigh, S. J. 2016. Energy Dispersive X-Ray Spectroscopy in Liquids: Inorganic and Biological Applications. Microscopy and Microanalysis, Vol. 22, Issue. S5, p. 72.
    Prestat, Eric Kulzick, Matthew A. Dietrich, Paul J. Doskocil, Eric Smith, Matthew Burke, M. Grace Haigh, Sarah J. and Zaluzec, Nestor J. 2016. European Microscopy Congress 2016: Proceedings. p. 17.
    De Yoreo, J. J. and N. A. J. M., Sommerdijk 2016. Investigating materials formation with liquid-phase and cryogenic TEM. Nature Reviews Materials, Vol. 1, Issue. 8,
    Download full list
    ×
  • Get access
    Add to cart USD35.00
    Check if you have access via personal or institutional login
    Log in Register Recommend to librarian

X-ray Energy-Dispersive Spectrometry During In Situ Liquid Cell Studies Using an Analytical Electron Microscope

  • Nestor J. Zaluzec (a1) (a2), M. Grace Burke (a2), Sarah J. Haigh (a2) and Matthew A. Kulzick (a3)
Abstract

The use of analytical spectroscopies during scanning/transmission electron microscope (S/TEM) investigations of micro- and nano-scale structures has become a routine technique in the arsenal of tools available to today’s materials researchers. Essential to implementation and successful application of spectroscopy to characterization is the integration of numerous technologies, which include electron optics, specimen holders, and associated detectors. While this combination has been achieved in many instrument configurations, the integration of X-ray energy-dispersive spectroscopy and in situ liquid environmental cells in the S/TEM has to date been elusive. In this work we present the successful incorporation/modifications to a system that achieves this functionality for analytical electron microscopy.

Copyright
© Microscopy Society of America 2014 
Corresponding author
* Corresponding author. Zaluzec@microscopy.com
References
Hide All
Chenna, S. & Crozer, P.A. (2011). Operando TEM—Detection of gas phase catalysis in an environmental TEM with EELS. Microsc Microanal 17(Suppl 2), 476–477.
Crewe, A.V. (1971). High resolution scanning microscopy of biological specimens. Philos Trans R Soc B 261, 61–70.
Crozer, P.A. & Chenna, S. (2011). In situ analysis of gas composition by electron energy-loss spectroscopy for environmental transmission electron microscopy. Ultramicroscopy 111, 177–185.
de Jonge, N. & Ross, F.M. (2011). Electron microscopy of specimens in liquid. Nat Nanotechnol 6, 695–704.
Egerton, R.F. (1986). Electron Energy Loss Spectroscopy. NewYork: Plenum Press.
Fraser, H.L., Klenov, D.O., Wang, Y.C., Cheng, H. & Zaluzec, N.J. (2011). On the performance of XEDS and EELS in the AEM: 25 years later. Microsc Microanal 17(Suppl 2), 590–591, doi:10.1017/S1431927611003825.
Holtz, M.E., Yu, Y., Gao, J., Abruña, H.D. & Muller, D.A. (2013). In situ electron energy-loss spectroscopy in liquids. Microsc Microanal 19, 1027–1035.
Howie, A. (1979). Image-contrast and localized signal selection techniques. J Microsc 117, 11–23.
Jungjohann, K.L., Evans, J.E., Aguiar, J.A., Arslan, I. & Browning, N.D. (2012). Atomic-scale imaging and spectroscopy for in situ liquid scanning transmission electron microscopy. Microsc Microanal 18, 621–627.
Liu, K.L., Wu, C.C., Huang, Y.J., Pang, H.L., Chang, H.Y., Chang, P., Hsu, L. & Yew, T.R. (2008). Novel microchip for in situ TEM imaging of living organisms and bio-reactions in aqueous conditions. Lab Chip 8, 1915–1921.
Malis, T., Cheng, S.C. & Egerton, R.F. (1988). EELS log-ratio technique for specimen-thickness measurement in the TEM. J Elec Micro Tech 8, 193–200.
Pennycook, S.J. (2012). Seeing the atoms more clearly: STEM imaging from the Crewe era to today. Ultramicroscopy 123, 28–37.
Ring, E.A. & de Jonge, N. (2010). Microfluidic system for transmission electron microscopy. Microsc Microanal 16, 622–629.
Symposium on New Opportunities for In-Situ (2013). New opportunities for in situ techniques and instruments. Microsc Microanal 19(Suppl 2), 392–476.
Williams, D.B. & Carter, C.B. (2009). Transmission Electron Microscopy: A Textbook for Materials Science. USA: Springer-Verlag.
Zaluzec, N.J. (1979). Introduction to Analytical Electron Microscopy. New York: Plenum Press, Chapter 4, 121–168.
Zaluzec, N.J. (2009). Detector solid angle formulas for use in X-ray energy dispersive spectrometry. Microsc Microanal 15, 93–98.
Recommend this journal

Email your librarian or administrator to recommend adding this journal to your organisation's collection.

Microscopy and Microanalysis
  • ISSN: 1431-9276
  • EISSN: 1435-8115
  • URL: /core/journals/microscopy-and-microanalysis
Please enter your name
Please enter a valid email address
Who would you like to send this to? *

CAPTCHA *

Skip to the audio challenge
×

Keywords:

Metrics

Full text views

Total number of HTML views: 7
Total number of PDF views: 165 *
Loading metrics...

Abstract views

Total abstract views: 564 *
Loading metrics...

* Views captured on Cambridge Core between September 2016 - 12th June 2018. This data will be updated every 24 hours.

Cancel
Confirm
×