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 Research described in this paper was performed at the Canadian Light Source, which is supported by the Canada Foundation for Innovation, Natural Sciences and Engineering Research Council of Canada, the University of Saskatchewan, the Government of Saskatchewan, Western Economic Diversification Canada, the National Research Council Canada, and the Canadian Institutes of Health Research. The authors acknowledge funding from NSERC and AREVA Resources Canada. We thank Lucia Zuin, Dongniu.Wang, Thasan Kandasamy, Erin Kope, and Erika Bergen for discussions and help with data collection. Trevor Flynn is thanked for data processing..