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Atomic-Scale Segregation and Fluctuations in Chemical Ordering FePt Thin Films

  • Karen L Torres (a1), Chandan Srivastava (a2), Richard L Martens (a3) and Gregory B Thompson (a4)

A series of atom probe and transmission electron microscopy (TEM) studies have been performed to quantify minute compositional fluctuations in Fe55Pt45 thin films during the A1 to L10 phase transformation. The atom probe specimens were analyzed in an Imago Local Electrode Atom Probe (LEAP®) at a target evaporation of 0.5%, a pulse fraction of 20% and a temperature of 120K. We noted a propensity of fracture failures in the LEAP with this material at lower temperatures. The atom probe reconstruction showed small levels of Pt segregation at grain boundaries in the as-deposited films. Fresnel-contrast TEM imaging confirmed high density fluctuations in these boundaries. Upon annealing at 600°C for 10 minutes, the film transformed from A1 to L10 and the grain boundaries become Fe enriched as compared to the as-deposited film.

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1. B Zhang and W.A. Soffa , Scripta Metallurgica 30 (6), 683 (1994).

2. M.F. Toney , W Lee , J.A. Hedstrom and A Kellock , Journal of Applied Physics 93 (12), 9902 (2003).

3. Y.K. Takahashi and K Hono , Scripta Materialia 53, 403 (2005).

4. K Thompson , D Lawrence , D.J. Larson , J.D. Olson , T.F Kelly and B Gorman , Ultramicroscopy 107, 131 (2007).

6. B. Yang , M Asta , O.N. Mryasov , T.J. Klemmer and R.W. Chantrell , Scripta Materialia 53, 417 (2005).

7. R.V. Chepulskii and W.H. Butler , Physical Review B 72, 134205 (2005).

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MRS Online Proceedings Library (OPL)
  • ISSN: -
  • EISSN: 1946-4274
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