Hostname: page-component-76fb5796d-r6qrq Total loading time: 0 Render date: 2024-04-25T14:39:44.856Z Has data issue: false hasContentIssue false
  • English
  • Français

Ratcheting behavior of ZEK100 magnesium alloy with various loading conditions and different immersing time

Published online by Cambridge University Press:  17 April 2017

Hong Gao ,
Wenbo Ye ,
Zhe Zhang  and
Lilan Gao
Hong Gao*
Affiliation:
School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, People’s Republic of China
Wenbo Ye
Affiliation:
School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, People’s Republic of China
Zhe Zhang
Affiliation:
School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, People’s Republic of China
Lilan Gao*
Affiliation:
School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, People’s Republic of China; and School of Mechanical Engineering, Tianjin University of Technology, Tianjin 300191, People’s Republic of China
*
a) Address all correspondence to this author. e-mail: gaolilan780921@163.com
Get access

Abstract

It is desirable to evaluate the ratcheting behavior of biomedical magnesium under cyclic loading with and without precorrosion, due to the promising future in biomedical implant field. This study focuses on the investigation of the uniaxial ratcheting strain evolutions of ZEK100 magnesium alloy sheet under various loading conditions and different corrosion time. To illustrate the ratcheting response in detail, the effects of several factors on the ratcheting strain evolution were discussed, including mean stress, stress amplitude, specimen orientations, loading history, and precorroded duration. A series of asymmetrical multistep stress-controlled ratcheting tests were conducted. The mean stress, stress amplitude, and precorrosion duration have significant influence on the ratcheting response of material. ZEK100 magnesium alloy is sensitive to loading history. ZEK100 magnesium alloy exhibits anisotropic behavior, and it is found that the final ratcheting strain of transverse direction (TD) specimens is always larger than that of rolling direction (RD) specimens. The corrosion behavior of ZEK100 magnesium alloy in phosphate buffered solution (PBS) simulated physiological environment was also studied. The corrosion process is characterized by pitting corrosion, and the corrosion rate of material stabilizes at about 2.4 g/(m2 d) after an exponentially decrease at initial stage.

Keywords

ZEK100Mg alloyratcheting straincorrosion behaviorloading historyprecorrodedstress/strain relationship
Type
Articles
Information
Journal of Materials Research , Volume 32 , Issue 11 , 14 June 2017 , pp. 2143 - 2152
Check for updates
Copyright
Copyright © Materials Research Society 2017 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Footnotes

Contributing Editor: Michele Manuel

References

REFERENCES

Witte, F., Fischer, J., Nellesen, J., Crostack, H.A., Kaese, V., Pisch, A., Beckmann, F., and Windhagen, H.: In vitro and in vivo corrosion measurements of magnesium alloys. Biomaterials 27, 1013 (2006).Google Scholar
Staiger, M.P., Pietak, A.M., Huadmai, J., and Dias, G.: Magnesium and its alloys as orthopedic biomaterials: A review. Biomaterials 27, 1728 (2006).Google Scholar
Shadanbaz, S., Walker, J., Staiger, M.P., Dias, G.J., and Pietak, A.: Growth of calcium phosphates on magnesium substrates for corrosion control in biomedical applications via immersion techniques. J. Biomed. Mater. Res., Part B 101, 162 (2013).Google Scholar
Zeng, R., Dietzel, W., Witte, F., Hort, N., and Blawert, C.: Progress and challenge for magnesium alloys as biomaterials. Adv. Eng. Mater. 10, B3 (2008).Google Scholar
Waizy, H., Weizbauer, A., Modrejewski, C., Witte, F., Windhagen, H., Lucas, A., Kieke, M., Denkena, B., Behrens, P., and Meyer-Lindenberg, A.: In vitro corrosion of ZEK100 plates in Hank’s balanced salt solution. Biomed. Eng. Online 11, 1 (2012).CrossRefGoogle ScholarPubMed
Gu, X.N., Zhou, W.R., Zheng, Y.F., Cheng, Y., Wei, S.C., Zhong, S.P., Xi, T.F., and Chen, L.J.: Corrosion fatigue behaviors of two biomedical Mg alloys—AZ91D and WE43—In simulated body fluid. Acta Biomater. 6, 4605 (2010).Google Scholar
Zhao, J., Gao, L.L., Gao, H., Yuan, X., and Chen, X.: Biodegradable behaviour and fatigue life of ZEK100 magnesium alloy in simulated physiological environment. Fatigue Fract. Eng. Mater. Struct. 38, 904 (2015).Google Scholar
Fu, S., Gao, H., Chen, G., Gao, L., and Chen, X.: Deterioration of mechanical properties for pre-corroded AZ31 sheet in simulated physiological environment. Mater. Sci. Eng., A 593, 153 (2014).Google Scholar
Lin, Y.C., Chen, X-M., Liu, Z-H., and Chen, J.: Investigation of uniaxial low-cycle fatigue failure behavior of hot-rolled AZ91 magnesium alloy. Int. J. Fatigue 48, 122 (2013).Google Scholar
Chen, X-M., Lin, Y.C., and Chen, J.: Low-cycle fatigue behaviors of hot-rolled AZ91 magnesium alloy under asymmetrical stress-controlled cyclic loadings. J. Alloys Compd. 579, 540 (2013).CrossRefGoogle Scholar
Lin, Y.C., Liu, Z-H., Chen, X-M., and Chen, J.: Stress-based fatigue life prediction models for AZ31B magnesium alloy under single-step and multi-step asymmetric stress-controlled cyclic loadings. Comput. Mater. Sci. 73, 128 (2013).Google Scholar
Lin, Y.C., Liu, Z-H., Chen, X-M., and Chen, J.: Uniaxial ratcheting and fatigue failure behaviors of hot-rolled AZ31B magnesium alloy under asymmetrical cyclic stress-controlled loadings. Mater. Sci. Eng., A 573, 234 (2013).Google Scholar
Ahmadzadeh, G.R. and Varvani-Farahani, A.: Triphasic ratcheting strain prediction of materials over stress cycles. Fatigue Fract. Eng. Mater. Struct. 35, 929 (2012).Google Scholar
Varvani-Farahani, A.: A comparative study in descriptions of coupled kinematic hardening rules and ratcheting assessment over asymmetric stress cycles. Fatigue Fract. Eng. Mater. Struct. (2016), doi: 10.1111/ffe.12549.Google Scholar
Xin, Y. and Chu, P.K.: In vitro studies of biomedical magnesium alloys in a simulated physiological environment: A review. Acta Biomater. 7, 1452 (2011).Google Scholar
Gao, H., Zhang, M., Zhao, J., Gao, L., and Li, M.: In vitro and in vivo degradation and mechanical properties of ZEK100 magnesium alloy coated with alginate, chitosan and mechano-growth factor. Mater. Sci. Eng., C 63, 450 (2016).Google Scholar
Sanchez, A.H.M., Luthringer, B.J.C., Feyerabend, F., and Willumeit, R.: Mg and Mg alloys: How comparable are in vitro and in vivo corrosion rates? A review. Acta Biomater. 13, 16 (2014).CrossRefGoogle Scholar
Staroselsky, A. and Anand, L.: A constitutive model for hcp materials deforming by slip and twinning: Application to magnesium alloy AZ31B. Int. J. Plast. 19, 1843 (2003).Google Scholar
Boba, M.: Warm forming behaviour of ZEK100 and AZ31B magnesium alloy sheet. Master's thesis, University of Waterloo, 2014.Google Scholar
Zhang, H., Dong, D.X., Ma, S.J., Gu, C.F., Chen, S., and Zhang, X.P.: Effects of percent reduction and specimen orientation on the ratcheting behavior of hot-rolled AZ31B magnesium alloy. Mater. Sci. Eng., A 575, 223 (2013).Google Scholar
Choi, S.H., Kim, D.H., Lee, H.W., Seong, B.S., Piao, K., and Wagoner, R.: Evolution of the deformation texture and yield locus shape in an AZ31 Mg alloy sheet under uniaxial loading. Mater. Sci. Eng., A 526, 38 (2009).Google Scholar
Bohlen, J., Nürnberg, M.R., Senn, J.W., Letzig, D., and Agnew, S.R.: The texture and anisotropy of magnesium–zinc–rare earth alloy sheets. Acta Mater. 55, 2101 (2007).CrossRefGoogle Scholar
Witte, F., Kaese, V., Haferkamp, H., Switzer, E., Meyer-Lindenberg, A., Wirth, C.J., and Windhagen, H.: In vivo corrosion of four magnesium alloys and the associated bone response. Biomaterials 26, 3557 (2005).Google Scholar
Dziuba, D., Meyer-Lindenberg, A., Seitz, J.M., Waizy, H., Angrisani, N., and Reifenrath, J.: Long-term in vivo degradation behaviour and biocompatibility of the magnesium alloy ZEK100 for use as a biodegradable bone implant. Acta Biomater. 9, 8548 (2013).Google Scholar
Song, G.L. and Atrens, A.: Corrosion mechanisms of magnesium alloys. Adv. Eng. Mater. 1, 11 (1999).3.0.CO;2-N>CrossRefGoogle Scholar
Yang, Z., Yuan, G., Zhang, X., Lin, M., Niu, J., and Ding, W.: Comparison of biodegradable behaviors of AZ31 and Mg–Nd–Zn–Zr alloys in Hank’s physiological solution. Mater. Sci. Eng., B 177, 395 (2012).Google Scholar
Witte, F., Hort, N., Vogt, C., Cohen, S., Kainer, K.U., Willumeit, R., and Feyerabend, F.: Degradable biomaterials based on magnesium corrosion. Curr. Opin. Solid State Mater. Sci. 12, 63 (2008).Google Scholar
Zhao, M.C., Liu, M., Song, G.L., and Atrens, A.: Influence of pH and chloride ion concentration on the corrosion of Mg alloy ZE41. Corros. Sci. 50, 3168 (2008).Google Scholar
Ambat, R., Aung, N.N., and Zhou, W.: Studies on the influence of chloride ion and pH on the corrosion and electrochemical behaviour of AZ91D magnesium alloy. J. Appl. Electrochem. 30, 865 (2000).Google Scholar
Song, G., Atrens, A., John, D.S., Wu, X., and Nairn, J.: The anodic dissolution of magnesium in chloride and sulphate solutions. Corros. Sci. 39, 1981 (1997).Google Scholar
Kang, G., Gao, Q., Cai, L., and Sun, Y.: Experimental study on uniaxial and nonproportionally multiaxial ratcheting of SS304 stainless steel at room and high temperatures. Nucl. Eng. Des. 216, 13 (2002).Google Scholar
Kang, G., Liu, Y., Wang, Y., Chen, Z., and Xu, W.: Uniaxial ratcheting of polymer and polymer matrix composites: Time-dependent experimental observations. Mater. Sci. Eng., A 523, 13 (2009).Google Scholar
Lin, Y.C., Chen, X.M., and Chen, G.: Uniaxial ratcheting and low-cycle fatigue failure behaviors of AZ91D magnesium alloy under cyclic tension deformation. J. Alloys Compd. 509, 6838 (2011).Google Scholar
Kishor, R., Sahu, L., Dutta, K., and Mondal, A.K.: Assessment of dislocation density in asymmetrically cyclic loaded non-conventional stainless steel using X-ray diffraction profile analysis. Mater. Sci. Eng., A 598, 299 (2014).Google Scholar
Ray, K.K., Dutta, K., Sivaprasad, S., and Tarafder, S.: Fatigue damage of AISI 304 LN stainless steel: Role of mean stress. Proc. Eng. 2, 1805 (2010).CrossRefGoogle Scholar
Yuan, X., Yu, D., Gao, L-L., and Gao, H.: Effect of phosphate-buffered solution corrosion on the ratcheting fatigue behavior of a duplex Mg–Li–Al alloy. J. Mater. Eng. Perform. 25, 1802 (2016).Google Scholar
Supplementary material: File

Gao supplementary material

Gao supplementary material 1

Download Gao supplementary material(File)
File 112.3 KB
Supplementary material: Image

Gao supplementary material

Fig. S1

Download Gao supplementary material(Image)
Image 488.8 KB