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AMS Radiocarbon Dating of Ancient Oriental Iron Artifacts at Nagoya University

Published online by Cambridge University Press:  18 July 2016

Toshio Nakamura
Affiliation:
Dating and Materials Research Center, Nagoya University, Chikusa, Nagoya 464-01 Japan
Masahiro Hirasawa
Affiliation:
School of Engineering, Nagoya University, Chikusa, Nagoya 464-01 Japan
Kenzo Igaki
Affiliation:
Faculty of Engineering, Tohoku University, Aoba, Sendai 980 Japan
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Abstract

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We present here the current status of AMS dating of iron artifacts at Nagoya University. We initially developed a “wet” method of carbon collection from iron samples, consisting of a resistance furnace and a “wet” trapping of the evolved CO2 with a saturated Ca(OH)2 solution, in which overall collection efficiency of carbon ranged from 50 to 60%. To improve the carbon-collection efficiency, we more recently constructed a “dry” system, consisting of an induction furnace followed by “dry” separation of the produced CO2 from combustion gases and conversion of the CO2 into a graphite target. We describe here mainly the performance of the “dry” separation system, tested using standard steel samples. We also report previously determined 14C dates on three ancient Oriental artifacts using the earlier “wet” procedure.

Type
V. Advances in Measurement Techniques
Copyright
Copyright © the Department of Geosciences, The University of Arizona 

References

Cresswell, R. G. 1991 The radiocarbon dating of iron artefacts using accelerator mass spectrometry. Historical Metallurgy 25: 7885.Google Scholar
Cresswell, R. G. 1992 Radiocarbon dating of iron artifacts. In Long, A. and Kra, R. S., eds., Proceedings of the 14th International 14C Conference. Radiocarbon 34(3): 898905.Google Scholar
Harbottle, G., Sayre, E. V. and Stoenner, R. W. 1979 Carbon-14 dating of small samples by proportional counters. Science 206: 683685.Google Scholar
Igaki, K., Nakamura, T., Hirasawa, M., Kato, M., and Sano, M. 1994 Radiocarbon dating study of ancient artifacts with accelerator mass spectrometry. Proceedings of the Japan Academy 70(B1): 49.CrossRefGoogle Scholar
Kitagawa, H., Masuzawa, T., Nakamura, T. and Matsumoto, E. 1993 A batch preparation method for graphite targets with low background for AMS 14C measurements. Radiocarbon 35(2): 295300.Google Scholar
Nakamura, T., Nakai, N., Sakase, T. Kimura, M., Ohishi, S., Taniguchi, M., and Yoshioka, S. 1985 Direct detection of radiocarbon using accelerator techniques and its application to age measurement. Japanese Journal of Applied Physics 24: 17161723.CrossRefGoogle Scholar
Nakamura, T., Nakazawa, T., Nakai, N., Kitagawa, H., Honda, H., Itoh, T., Machida, T. and Matsumoto, E. 1992 Measurement of 14C concentrations of stratospheric CO2 by accelerator mass spectrometry. In Long, A. and Kra, R. S., eds., Proceedings of the 14th International 14C Conference. Radiocarbon 34(3): 745752.CrossRefGoogle Scholar
Niklaus, T. R. 1991 CalibETH 1.5b, Program for calibration of radiocarbon dates. Institute for Intermediate Energy Physics, ETH, Zurich, Switzerland.Google Scholar
Niklaus, T. R., Bonani, G., Simonius, M., Suter, M. and Wolfli, W. 1992 CalibETH: An interactive computer program for the calibration of radiocarbon dates. In Long, A. and Kra, R. S., eds., Proceedings of the 14th International 14C Conference. Radiocarbon 34(3): 483492.Google Scholar
Sayre, E. V., Harbottle, G., Stoenner, R. W., Washburn, W., Olin, J. S. and Fitzhugh, W. W. 1982 The carbon-14 dating of an iron bloom associated with the voyages of Sir Martin Frobisher. American Chemical Society Symposium Series 176: 441451.CrossRefGoogle Scholar
Stuiver, M. and Pearson, G. W. 1993 High-precision bidecadal calibration of the radiocarbon time scale, ad 1950–500 bc and 2500–6000 bc. In Stuiver, M., Long, A. and Kra, R.S., eds., Calibration 1993. Radiocarbon 35(1): 123.Google Scholar
van der Merwe, N. J. and Stuiver, M. 1968 Dating iron by the carbon-14 method. Current Anthropology 9: 4853.CrossRefGoogle Scholar
Yoshida, K. 1992 Measurement of 14C age by accelerator mass spectrometry. Bulletin of the National Museum of Japanese History 38: 171198.Google Scholar