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One-step Solvothermal Synthesis and Characterization of BaTiO3 Nanoparticles

Published online by Cambridge University Press:  15 February 2011

Helen Reveron ,
Cyril Aymonier ,
Anne Loppinet-Serani ,
Mario Maglione ,
Catherine Elissalde  and
Francois Cansell
Helen Reveron
Affiliation:
Catherine Elissalde and Francois Cansell Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB), 87 Av. du Dr. Schweitzer, 33608 Pessac, France.
Cyril Aymonier
Affiliation:
Catherine Elissalde and Francois Cansell Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB), 87 Av. du Dr. Schweitzer, 33608 Pessac, France.
Anne Loppinet-Serani
Affiliation:
Catherine Elissalde and Francois Cansell Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB), 87 Av. du Dr. Schweitzer, 33608 Pessac, France.
Mario Maglione
Affiliation:
Catherine Elissalde and Francois Cansell Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB), 87 Av. du Dr. Schweitzer, 33608 Pessac, France.
Catherine Elissalde
Affiliation:
Catherine Elissalde and Francois Cansell Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB), 87 Av. du Dr. Schweitzer, 33608 Pessac, France.
Francois Cansell
Affiliation:
Catherine Elissalde and Francois Cansell Institut de Chimie de la Matière Condensée de Bordeaux (ICMCB), 87 Av. du Dr. Schweitzer, 33608 Pessac, France.
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Abstract

Using a continuous-flow reactor, barium titanate (BaTiO3) nanoparticles have been successfully synthesized at temperatures ranging from 150 to 380°C and 16 MPa. Ba-Ti alkoxide solutions were used as precursors and water as reagent. The influence of synthesis parameters on the powder characteristics was investigated. Results showed that the purity, crystallinity and stoichiometry of the as-synthesized BaTiO3 powder depend mainly on the reactor temperature, quantity of water injected into the reactor and the Ba:Ti molar ratio of alkoxide solutions.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 878: Symposium Y – Solvothermal Synthesis and Processing of Materials , 2005 , Y1.5
Copyright
Copyright © Materials Research Society 2005

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