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A comparative investigation of long-term oxidation behavior of selective laser melting–fabricated Inconel 718 at 650 °C

Published online by Cambridge University Press:  26 May 2020

Yan-Wen Luo ,
Bin Zhang Open the ORCID record for Bin Zhang [Opens in a new window] ,
Zhu-Man Song ,
Chang-Peng Li ,
Guo-Feng Chen  and
Guang-Ping Zhang Open the ORCID record for Guang-Ping Zhang [Opens in a new window]
Yan-Wen Luo
Affiliation:
Key Laboratory for Anisotropy and Texture of Materials, Ministry of Education, School of Materials Science and Engineering, Northeastern University, Shenyang 110819, People's Republic of China; and Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
Bin Zhang*
Affiliation:
Key Laboratory for Anisotropy and Texture of Materials, Ministry of Education, School of Materials Science and Engineering, Northeastern University, Shenyang 110819, People's Republic of China
Zhu-Man Song
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
Chang-Peng Li
Affiliation:
Materials & Manufacturing Qualification Group, Corporate Technology, Siemens Ltd., China, Beijing 100102, People's Republic of China
Guo-Feng Chen
Affiliation:
Materials & Manufacturing Qualification Group, Corporate Technology, Siemens Ltd., China, Beijing 100102, People's Republic of China
Guang-Ping Zhang*
Affiliation:
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, People's Republic of China
*
a)Address all correspondence to these authors. e-mail: zhangb@atm.neu.edu.cn
b)e-mail: gpzhang@imr.ac.cn
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Abstract

The oxidation behavior of the selective laser melting (SLM)–fabricated Inconel 718 was investigated through isothermal oxidation testing at 650 °C for 500 h and compared with that of the as-cast and as-forged specimens at the same testing conditions. The effect of microstructure and surface roughness on the oxidation behavior of the SLM-fabricated, as-cast, and as-forged Inconel 718 specimens was examined. The result shows that Inconel 718 fabricated by SLM with the unique layer structure exhibited a better resistance to the 500 h oxidation at 650 °C compared with as-cast and as-forged 718 with coarse dendritic structure and uniform equiaxed grain microstructure, respectively. The influence of the surface roughness on the long-time oxidation resistance of SLM specimens is not pronounced compared with that of as-cast and as-forged specimens. The tiny dendrites instead of grain boundaries are a major influencing factor for the oxidation process of SLM specimens. The surface roughness has more evident influence on the oxidation resistance of as-forged specimens than that of the as-cast ones subjected to the 500 h oxidation at 650 °C.

Keywords

oxidationalloymicrostructure
Type
Article
Information
Journal of Materials Research , Volume 35 , Issue 15: Focus Issue: Additive Manufacturing of Metals: Complex Microstructures and Architecture Design , 14 August 2020 , pp. 2036 - 2045
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Copyright © Materials Research Society 2020

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References

Yadollahi, A. and Shamsaei, N.: Additive manufacturing of fatigue resistant materials: Challenges and opportunities. Int. J. Fatig. 98, 14 (2017).CrossRefGoogle Scholar
DebRoy, T., Wei, H.L., Zuback, J.S., Mukherjee, T., Elmer, J.W., Milewski, J.O., Beese, A.M., Wilson-Heid, A., De, A., and Zhang, W.: Additive manufacturing of metallic components—Process, structure, and properties. Prog. Mater. Sci. 92, 112 (2018).CrossRefGoogle Scholar
Wang, X., Gong, X., and Chou, K.: Review on powder-bed laser additive manufacturing of Inconel 718 parts. Proc. Inst. Mech. Eng., Part B 231, 1890 (2016).CrossRefGoogle Scholar
Romano, J., Ladani, L., and Sadowski, M.: Laser additive melting and solidification of Inconel 718: Finite element simulation and experiment. JOM 68, 967 (2016).CrossRefGoogle Scholar
Lewandowski, J.J. and Seifi, M.: Metal additive manufacturing: A review of mechanical properties. Annu. Rev. Mater. Res. 46, 151 (2016).10.1146/annurev-matsci-070115-032024CrossRefGoogle Scholar
Wang, X. and Chou, K.: Effects of thermal cycles on the microstructure evolution of Inconel 718 during selective laser melting process. Addit. Manuf. 18, 1 (2017).Google Scholar
Amato, K.N., Gaytan, S.M., Murr, L.E., Martinez, E., Shindo, P.W., Hernandez, J., Collins, S., and Medina, F.: Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting. Acta Mater. 60, 2229 (2012).CrossRefGoogle Scholar
Mukherjee, T. and DebRoy, T.: A digital twin for rapid qualification of 3D printed metallic components. Appl. Mater. Today 14, 59 (2019).CrossRefGoogle Scholar
Kok, Y., Tan, X.P., Wang, P., Nai, M.L.S., Loh, N.H., Liu, E., and Tor, S.B.: Anisotropy and heterogeneity of microstructure and mechanical properties in metal additive manufacturing: A critical review. Mater. Des. 139, 565 (2018).CrossRefGoogle Scholar
Deng, D., Peng, R.L., Brodin, H., and Moverare, J.: Microstructure and mechanical properties of Inconel 718 produced by selective laser melting: Sample orientation dependence and effects of post heat treatments. Mater. Sci. Eng., A 713, 294 (2018).CrossRefGoogle Scholar
Rezende, M.C., Araújo, L.S., Gabriel, S.B., Dille, J., and de Almeida, L.H.: Oxidation assisted intergranular cracking under loading at dynamic strain aging temperatures in Inconel 718 superalloy. J. Alloys Compd. 643, S256 (2015).CrossRefGoogle Scholar
Huang, L., Sun, X.F., Guan, H.R., and Hu, Z.Q.: Effect of rhenium addition on isothermal oxidation behavior of single-crystal Ni-based superalloy. Surf. Coat. Technol. 200, 6863 (2006).10.1016/j.surfcoat.2005.10.037CrossRefGoogle Scholar
Sato, A., Chiu, Y.L., and Reed, R.C.: Oxidation of nickel-based single-crystal superalloys for industrial gas turbine applications. Acta Mater. 59, 225 (2011).10.1016/j.actamat.2010.09.027CrossRefGoogle Scholar
Weng, F., Yu, H., Chen, C., and Wan, K.: High-temperature oxidation behavior of Ni-based superalloys with Nb and Y and the interface characteristics of oxidation scales. Surf. Interface Anal. 47, 362 (2015).CrossRefGoogle Scholar
Greene, G.A. and Finfrock, C.C.: Oxidation of Inconel 718 in air at high temperatures. Oxid. Met. 55, 505 (2001).CrossRefGoogle Scholar
Geng, L., Na, Y-S., and Park, N-K.: Oxidation behavior of alloy 718 at a high temperature. Mater. Des. 28, 978 (2007).CrossRefGoogle Scholar
Omidbakhsh, F., Ebrahimi, A.R., and Sojka, J.: High temperature oxidation effects on surface roughness of Ti–4Al–2V. Surf. Eng. 29, 322 (2013).CrossRefGoogle Scholar
Wang, X., Fan, F., Szpunar, J.A., and Zhang, L.: Influence of grain orientation on the incipient oxidation behavior of Haynes 230 at 900 °C. Mater. Charact. 107, 33 (2015).CrossRefGoogle Scholar
Caplan, D. and Sproule, G.: Effect of oxide grain structure on the high-temperature oxidation of Cr. Oxid. Met. 9, 459 (1975).CrossRefGoogle Scholar
Juillet, C., Oudriss, A., Balmain, J., Feaugas, X., and Pedraza, F.: Characterization and oxidation resistance of additive manufactured and forged IN718 Ni-based superalloys. Corros. Sci. 142, 266 (2018).CrossRefGoogle Scholar
Balat-Pichelin, M., Sans, J.L., Bêche, E., Flaud, V., and Annaloro, J.: Oxidation and emissivity of Inconel 718 alloy as potential space debris during its atmospheric entry. Mater. Charact. 127, 379 (2017).CrossRefGoogle Scholar
Zhang, Y.N., Cao, X., Wanjara, P., and Medraj, M.: Oxide films in laser additive manufactured Inconel 718. Acta Mater. 61, 6562 (2013).CrossRefGoogle Scholar
Zielińska, M., Sieniawski, J., Yavorska, M., and Motyka, M.: Influence of chemical composition of nickel based superalloy on the formation of aluminide coatings. Arch. Metall. Mater. 56, 193 (2011).CrossRefGoogle Scholar
Jia, Q. and Gu, D.: Selective laser melting additive manufacturing of Inconel 718 superalloy parts: Densification, microstructure, and properties. J. Alloys Compd. 585, 713 (2014).CrossRefGoogle Scholar
Hong, J.K., Park, N.K., Kim, S.J., and Kang, C.Y.: Microstructures of oxidized primary carbides on superalloy Inconel 718. Materials Science Forum Masaaki Naka and Toshimi Yamane 502, 249 2005.Google Scholar
Zhang, H., Li, C., Guo, Q., Ma, Z., Huang, Y., Li, H., and Liu, Y.: Hot tensile behavior of cold-rolled Inconel 718 alloy at 650 °C: The role of δ phase. Mater. Sci. Eng., A 722, 136 (2018).CrossRefGoogle Scholar
Anderson, M., Thielin, A.L., Bridier, F., Bocher, P., and Savoie, J.: δ phase precipitation in Inconel 718 and associated mechanical properties. Mater. Sci. Eng., A 679, 48 (2017).CrossRefGoogle Scholar
Azadian, S., Wei, L-Y., and Warren, R.: Delta phase precipitation in Inconel 718. Mater. Charact. 53, 7 (2004).CrossRefGoogle Scholar
Kang, Y-J., Yang, S., Kim, Y-K., AlMangour, B., and Lee, K-A.: Effect of post-treatment on the microstructure and high-temperature oxidation behaviour of additively manufactured Inconel 718 alloy. Corros. Sci. 158, 108082 (2019).CrossRefGoogle Scholar
Jia, Q. and Gu, D.: Selective laser melting additive manufactured Inconel 718 superalloy parts: High-temperature oxidation property and its mechanisms. Optic Laser. Technol. 62, 161 (2014).CrossRefGoogle Scholar
Bai, Y., Hua, Y., Rong, Z., Ye, Y., Xue, Q., Liu, H., and Chen, R.: Cyclic oxidation resistance of In718 superalloy treated by laser peening. J. Wuhan Univ. Technol., Mater. Sci. Ed. 30, 808 (2015).CrossRefGoogle Scholar
Jayaraj, J., Thirathipviwat, P., Han, J., and Gebert, A.: Microstructure, mechanical, and thermal oxidation behavior of AlNbTiZr high entropy alloy. Intermetallics 100, 9 (2018).CrossRefGoogle Scholar
Harun, W.S.W., Asri, R.I.M., Romlay, F.R.M., Sharif, S., Jan, N.H.M., and Tsumori, F.: Surface characterisation and corrosion behaviour of oxide layer for SLMed-316L stainless steel. J. Alloys Compd. 748, 1044 (2018).CrossRefGoogle Scholar
Mobini, S., Meshkani, F., and Rezaei, M.: Surfactant-assisted hydrothermal synthesis of CuCr2O4 spinel catalyst and its application in CO oxidation process. J. Chem. Environ. Eng. 5, 4906 (2017).CrossRefGoogle Scholar
Karlsson, J., Norell, M., Ackelid, U., Engqvist, H., and Lausmaa, J.: Surface oxidation behavior of Ti–6Al–4V manufactured by electron beam melting (EBM®). J. Manuf. Process. 17, 120 (2015).10.1016/j.jmapro.2014.08.005CrossRefGoogle Scholar
Sanviemvongsak, T., Monceau, D., and Macquaire, B.: High temperature oxidation of IN 718 manufactured by laser beam melting and electron beam melting: Effect of surface topography. Corros. Sci. 141, 127 (2018).CrossRefGoogle Scholar
Wang, L., Jiang, W-G., Li, X-W., Dong, J-S., Zheng, W., Feng, H., and Lou, L-H.: Effect of surface roughness on the oxidation behavior of a directionally solidified Ni-based superalloy at 1100 °C. Acta Metall. Sin. 28, 381 (2015).CrossRefGoogle Scholar
Rybicki, G.C. and Smialek, J.L.: Effect of the θ-α-Al2O3 transformation on the oxidation behavior of β-NiAl+Zr. Oxid. Met. 31, 275 (1989).CrossRefGoogle Scholar
Luo, Y.W., Zhang, B., Li, C.P., Chen, G.F., and Zhang, G.P.: Detecting void-induced scatter of fatigue life of selective laser melting-fabricated Inconel 718 using miniature specimens. Mater. Res. Express 6, 046549 (2019).CrossRefGoogle Scholar
Zhai, Y., Galarraga, H., and Lados, D.A.: Microstructure evolution, tensile properties, and fatigue damage mechanisms in Ti–6Al–4V alloys fabricated by two additive manufacturing techniques. Procedia Eng. 114, 658 (2015).CrossRefGoogle Scholar
Mumtaz, K. and Hopkinson, N.: Top surface and side roughness of Inconel 625 parts processed using selective laser melting. Rapid Prototyp. J. 15, 96 (2009).CrossRefGoogle Scholar
Evans, J.L.: Effect of surface roughness on the oxidation behavior of the Ni-base superalloy ME3. J. Mater. Eng. Perform. 19, 1001 (2010).10.1007/s11665-010-9605-5CrossRefGoogle Scholar
Zhao, H., Song, H., Xu, L., and Chou, L.: Isobutane dehydrogenation over the mesoporous Cr2O3/Al2O3 catalysts synthesized from a metal-organic framework MIL-101. Appl. Catal., A 456, 188 (2013).CrossRefGoogle Scholar
Dressler, M., Nofz, M., Dörfel, I., and Saliwan-Neumann, R.: Diffusion of Cr, Fe, and Ti ions from Ni-base alloy Inconel-718 into a transition alumina coating. Thin Solid Films 520, 4344 (2012).CrossRefGoogle Scholar
Strößner, J., Terock, M., and Glatzel, U.: Mechanical and microstructural investigation of nickel‐based superalloy IN718 manufactured by selective laser melting (SLM). Adv. Eng. Mater. 17, 1099 (2015).CrossRefGoogle Scholar
Zhang, X., Wang, Z., Lin, J., and Zhou, Z.: A study on high temperature oxidation behavior of high-velocity arc sprayed Fe-based coatings. Surf. Coat. Technol. 283, 255 (2015).CrossRefGoogle Scholar
Peng, Y., Zhang, C., Zhou, H., and Liu, L.: On the bonding strength in thermally sprayed Fe-based amorphous coatings. Surf. Coat. Technol. 218, 17 (2013).CrossRefGoogle Scholar
Sergeant, D.: Scale Formation and Adhesion to Mild Steels during Reheating for Hot Working (Sheffield Hallam University, Sheffield, UK. 1974). Available from Sheffield Hallam University Research Archive (SHURA) at: http://shura.shu.ac.uk/20343/Google Scholar
Meier, G.: Research on oxidation and embrittlement of intermetallic compounds in the US. Mater. Corros. 47, 595 (1996).CrossRefGoogle Scholar
Liu, Y., Wu, Y., Wang, J., and Ning, Y.: Oxidation behavior and microstructure degeneration of cast Ni-based superalloy M951 at 900 °C. Appl. Surf. Sci. 479, 709 (2019).CrossRefGoogle Scholar
Walmsley, J.C., Albertsen, J.Z., Friis, J., and Mathiesen, R.H.: The evolution and oxidation of carbides in an Alloy 601 exposed to long term high temperature corrosion conditions. Corros. Sci. 52, 4001 (2010).CrossRefGoogle Scholar