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Microwave Sintering of Large Products

Published online by Cambridge University Press:  10 February 2011

Tasaburo Saji*
Affiliation:
Fujidempa Kogyo Co., LTD. Tsukuba Laboratory Ibaraki Japan
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Abstract

A practical microwave ceramic sintering technology has been developed. To achieve the highest merit from microwave sintering, susceptors were not used. In this paper, the ceramic sintering process using the 28GHz mm-wave energy generated by a Gyrotron oscillator is described. Large sized (Φ 200 × 200 ) and complex shaped material of Si3N4, A12O3, and ZrO2 were successfully and reproducibly sintered. The sintered bodies exhibited high density and fine crystalline structure. The processed materials were found to have exceptional strength and toughness.

The critical processing technology developed dealt with the means by which uniform and defect free sintered bodies are obtained. The processing stressed the importance of achieving a uniform electric field within the applicator and to decrease the sintering dependence on the materials’ temperature based dielectric loss properties. With the use of innovative support and thermal insulation structures, the processing system allowed for very precise temperature controls.

Type
Research Article
Copyright
Copyright © Materials Research Society 1996

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References

1. Sutton, W.H., “Microwave processing of Ceramics-an Overview “Materials Research Society Symposium Proceedings Vol.269, Microwave Processing of Materials (1992) 23 Google Scholar
2. Tiegs, T.N., Kiggans, J.O. and Kimrey, H.D., “Microwave Sintering of Silicon Nitride” Ceramic Engineering Society proceedings 12 (1991)Google Scholar
3. Kimrey, H.D., Kiggans, J.O., Janney, M.A., Beatty, R.L., “Microwave Sintering of Zirconia-Toughened Alumina Composites” Materials Research Society Symposium proceedings Vol. 189 P 243255 (1991)Google Scholar
4. Saji, T., “Mechanism of Microwave Sintering, and Millimeter Wave Sintering” New Ceramics Vol. 8, No, 5 P 21 (1995)Google Scholar