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Synthesis of AlFe Intermetallic Nanoparticles by High-Energy Ball Milling

Published online by Cambridge University Press:  12 May 2015

G. Rosas ,
J. Chihuaque ,
E. Bedolla ,
R. Esparza  and
R. Pérez
G. Rosas
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, Morelia, Mich., 58000, México. *Email: grtrejo@umich.mx
J. Chihuaque
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, Morelia, Mich., 58000, México. *Email: grtrejo@umich.mx
E. Bedolla
Affiliation:
Instituto de Investigaciones Metalúrgicas, UMSNH, Edificio U, Ciudad Universitaria, Morelia, Mich., 58000, México. *Email: grtrejo@umich.mx
R. Esparza
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, Santiago de Querétaro, Qro., 76230, México.
R. Pérez
Affiliation:
Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, Santiago de Querétaro, Qro., 76230, México.
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Abstract

In this investigation, the chemical and microstructural characteristics of nanostructured AlFe intermetallic produced by high-energy ball milling have been explored. High purity elemental powders were used as the starting material. The ball milling was carried out at room temperature using a SPEX-8000 mixer/mill. The structure, morphology and compositions of the powders were obtained using X-ray diffraction patterns (XRD), scanning and transmission electron microscopy (STEM). High resolution electron microscopy observations have been used in the nanostructured materials characterization. The structural configurations have been explored through comparisons between experimental HREM images and theoretically simulated images obtained with the multislice method of the dynamical theory of electron diffraction.

Keywords

NanostructureAlScanning Electron Microscopy (SEM)Transmission Electron Microscopy (TEM)X-ray diffraction (XRD)
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1766: Symposium 5B – Structural and Chemical Characterization of Metals, Alloys, and Compounds—2014 , 2015 , pp. 181 - 186
Copyright
Copyright © Materials Research Society 2015 

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