An assumption exists in North Alaskan archaeological literature that radiometric assays produced by the now-defunct Dicarb Radioisotope Co. (Dicarb) are “too young” or more recent when compared to those produced by other laboratories. This assumption is statistically tested by comparing radiocarbon assays produced by Dicarb to those produced by Beta Analytic, Inc.; Geochron Laboratories; and the NSF-Arizona AMS Facility. The primary data set consists of radiometric and accelerator mass spectrometry (AMS) assays produced from materials excavated at the Croxton site, Locality J, Tukuto Lake, northern Alaska. Statistical analyses demonstrate that 14C assays produced by Dicarb tend to be “younger” than assays produced by other laboratories on crosscheck samples, with differences ranging between 350 and 1440 yr.

It is difficult to construct archaeological chronologies for Babeldaob, the main island of Palau (western Micronesia), because the saprolitic clays of the dominant terraced-hill sites and associated ceramic sherds often contain old carbon that originated in lignites. This has implications, as well, for chronologies of sedimentary sequences. Comparative analysis of the dating problem using lignite, pottery, and charcoal samples indicates that, in fact, there are both old and young sources of potential contamination. It is concluded that radiocarbon samples from Babeldaob need to be tested for appropriate carbon content rather than relying solely upon material identification.

California's San Miguel Island contains over 600 archaeological sites, some occupied as early as 12,000 yr ago and most located along the island's north coast. Archaeologists have long believed the south coast to have been marginal or largely uninhabited. Burial of some landforms by sand dunes deposited after historical overgrazing, the lack of systematic survey, and a dearth of radiocarbon dating have also contributed to an underestimation of the intensity of human land use along the south coast of San Miguel Island. Our recent reconnaissance and dating of shell middens on the island's south coast indicate more intensive occupation than previously thought, with numerous south coast sites spanning at least the past 9000 yr, and demonstrate the utility of combining systematic archaeological reconnaissance and radiometrics in reconstructions of human settlement and historical ecology in coastal environments.

Accelerator mass spectrometry (AMS) determinations of rat bones from natural and cultural sites in New Zealand have produced ages at odds with the accepted date for early human settlement by over 1000 yr. Since rats are a human commensal, this implies either an earlier visitation by people or problems with the reliability of the AMS determinations. One explanation for the extreme ages is dietary variation involving movement of depleted radiocarbon through dietary food chains to rats. To investigate this, we 14C dated fauna from the previously well-dated site of Shag River Mouth. The faunal remains were of species that consumed carbon derived from a variety of environments within the orbit of the site, including the estuary, river, land, and sea. The 14C results showed a wide range in age among estuarine and freshwater species. Terrestrial and marine organisms produced ages within expectations. We also found differences between bone dated using the Oxford ultrafiltration method and those treated using the filtered gelatin method. This implies that contamination could also be of greater importance than previously thought.

In archaeological dating, the greatest confidence is usually placed upon radiocarbon results of material that can be directly related to a defined archaeological event. Human bone should fulfill this requirement, but bone dates obtained from Pacific sites are often perceived as problematic due to the incorporation of 14C from a range of different reservoirs into the collagen via diet. In this paper, we present new human bone gelatin results for 2 burials from the SAC archaeological site on Watom Island, Papua New Guinea, and investigate the success of calibrating these determinations using dietary corrections obtained from δ34S, δ15N, and δ13C isotopes.

Radiocarbon dating of early Pre-Pottery Neolithic B (PPNB) deposits at the site of Motza, Israel, was achieved by first prescreening many charcoal and bone samples in order to identify those that are in the most suitable state of preservation for dating. For assessing bone preservation, we determined the collagen contents, and by infrared spectroscopy the collagen purity. The collagen samples of the best preserved bones were then further characterized by their C/N ratios and amino acid compositions. Prescreening of the charcoal samples involved monitoring the changes in infrared and Raman spectra during the acid-alkali-acid treatments. In some samples, we noted that the clay content increased with additional alkali treatments. These samples were rejected, as this could result in erroneous dates. No differences were observed in the 14C dates between charcoal and bone collagen samples. The dates range from 10,600–10,100 cal BP, which is consistent with dates for the early PPNB from other sites. This is of much interest in terms of better understanding where and when domestication of animals began in this period, and how agriculture spread throughout the Levant.

Direct accelerator mass spectrometry (AMS) dating of anaerobically preserved plant remains from the Dongan site in New Guinea, combined with assessment of preservation condition, confirms earlier doubts about the antiquity of betelnut (Areca catechu L.) found at the site. A possible sago leaf fragment is also identified as a modern contaminant. The mid-Holocene age of other fruit and nut remains is verified using these methods. The utility of AMS dating in combination with detailed archaeobotanical assessment is demonstrated, thus improving chronometric hygiene and with it knowledge of past plant use in Oceania.

Xinzhai is an important archaeological site discovered 40 yr ago and recently re-excavated in the Henan Province, China. It is believed that the cultural characteristics of the Xinzhai site correspond to the Xia dynasty, the first ancient dynasty of China. Radiocarbon measurements on bone samples from this site were performed at the Peking University AMS facility (PKU-AMS) and the Vienna University AMS facility (VERA). Calibrated ages were obtained with the computer program OxCal. The results of these measurements are presented and the related chronology is discussed.

Radiocarbon dates together with geoarchaeological, soil, and lithic analyses are presented to describe archaeological site 35-CS-9 in Bandon Ocean Wayside State Park, Oregon, northwestern USA. One of the few Oregon middle-Holocene coastal sites that includes sediments and artifacts dating to the early Holocene and possibly to the late Pleistocene, it was recorded in 1951 and surface surveyed by archaeologists in 1975, 1986, and 1991, but its depth and antiquity were not tested. In February 2002, we studied the site's stratigraphy and sediments and described 8 strata from the aeolian surface to bedrock at 350 cm depth. Soil samples taken from a cut bank for texture classification, particle size analysis, pH, carbon content, and chemical analysis suggested that the site represented a complete history of Holocene deposits. Excavation of 2 test units in August 2002 uncovered substantial lithic and charcoal remains that confirm a protracted middle-Holocene occupation and suggest that human occupation began in the early Holocene. Charcoal recovered at 235–245 cm dated to 11,000 14C BP, and the deepest lithic artifact was recovered in a level at 215–225 cm. Whether the human occupation was continuous throughout the Holocene, and whether it began in the early Holocene or in the late Pleistocene, can only be determined with further excavations.

Bone and charcoal samples from the Neolithic site of Serra Cicora in the Salento Peninsula (southern Italy) have been dated by accelerator mass spectrometry (AMS). Measurements appear to support other archaeological evidence and have shown that 2 distinct phases of human occupation of the site can be identified: the first occupation in the Early Neolithic and a second occupation in the Middle-Late Neolithic. The results provide new information and are a fundamental contribution to the definition of the absolute chronology of the Middle-Late Neolithic in this part of Europe.

The “bomb” radiocarbon spike induced by atmospheric nuclear detonations has been reconstructed at a latitude of 40°N by measuring the 14C content in annual rings of a living pine (Pinus pinea) at the Accelerator Mass Spectrometry facility of the University of Lecce. We report how the samples were taken, selected, prepared for analysis, and measured. The results are in good agreement with other data sets available for the Northern Hemisphere temperate regions, showing that a curve for the calibration of 14C dates, valid for the whole Northern Hemisphere, can be established for the second half of the 20th century.

Radioactive nuclides such as radiocarbon can be good tracers for investigating the circulation of underground carbon and water. Volcanic gas can be sampled reliably for 14C analysis and prepared for analysis by accelerator mass spectrometry (AMS). In this paper, we establish a method for the measurement of 14C in volcanic gas, and measure the amounts of 14C in various volcanic gases. Samples of fumarolic gas from some Japanese volcanoes were found to contain 0.5 to 4.2 pMC, while those from White Island in New Zealand contained 2.6 pMC. Dissolved gas from Lake Nyos, Cameroon, contained 0.4 to 4.8 pMC. The data indicate a mixing process between surface carbon and deep carbon.

A new method is presented for the reconstruction of the radiocarbon production rate from the measured relative abundance of Δ14C. The method treats the carbon cycle as a linear Fourier filter and thus allows for the correct and unambiguous inversion of the carbon cycle. The 14C production rate, as reconstructed by the Fourier filter method, agrees with the results obtained by the traditional iteration method. Since the 2 methods use completely different approaches, this verifies the validity of the reconstruction. The composite series is presented, based on both methods and their systematic uncertainties.