Hostname: page-component-848d4c4894-75dct Total loading time: 0 Render date: 2024-05-20T22:23:45.535Z Has data issue: false hasContentIssue false

Measurement of Thickness of Dispersed Clay Flakes with the Electron Microscope

Published online by Cambridge University Press:  01 January 2024

A. H. Weir
Affiliation:
Rothamsted Experimental Station, Harpenden, England
H. L. Nixon
Affiliation:
Rothamsted Experimental Station, Harpenden, England
R. D. Woods
Affiliation:
Rothamsted Experimental Station, Harpenden, England

Abstract

The shadow lengths of dispersed flakes of the layer-lattice mineral, allevardite, were measured with the electron microscope. Details of the experimental technique are given, and the importance of using samples free from very small material is stressed. Measurements of flake thickness made in this way agree well with estimates of the basal spacing of the collapsed lattice obtained from X-ray diffraction, and dispersion of allevardite was found to produce suspended flakes 19 Å thick, corresponding in thickness to the basic structural unit of two 2:1 layers.

Type
General Session
Copyright
Copyright © The Clay Minerals Society 1960

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Bachmann, L., Orr, W. H., Rhodin, T. N. and Siegel, B. M. (1960) Determination of surface structure using ultra high vacuum replication: J. Appl. Phys., v. 31, pp. 14581463.CrossRefGoogle Scholar
Bates, T. F. (1958) Selected electron micrographs of clays and other fine-grained materials: Mineral Industries Exp. Sta., Penn. State University, Circular 51, p. 61.Google Scholar
Bradley, D. E. (1954) Evaporated carbon films for electron microscopy: Brit. J. Appl. Phys., v. 5, pp. 6566.CrossRefGoogle Scholar
Brindley, G. W. (1956) Allevardite, a swelling double-layer mica mineral: Amer. Min., v. 41, pp. 93103.Google Scholar
Caillère, S., Mathieu-Sicaud, A. and Hénin, S. (1950) Nouvel essai d'identification du mineral de La Table près Allevard, l'allevardite: Bull. Soc. Franç. Min., v. 73, pp. 193201.Google Scholar
Grim, B. E. (1953) Clay Mineralogy, p. 116 McGraw-Hill Book Co., Inc., New York, 384 pp.Google Scholar
Hénin, S., Esquevin, J., and Caillère, S., (1954) Sur la fibrosité de certains minéraux de nature montmorillonitique: Bull. Soc. Franç. Min., v. 77, pp. 491499.Google Scholar
Ivkin, N. M., Kitaigorodski, N. S., Kotelnikov, D. D. and Korolyev, U. M. (1959) An analogue of allevardite (from Dagestan): Notes of the All-Union Mineralogical Society, ser. 2, p. 88, Issue 5, pp. 554-563.Google Scholar
Nixon, H. L. and Fisher, H. L. (1958) An improved spray droplet technique for quantitative electron microscopy: Brit. J. Appl. Phys., v. 9, pp. 6870.CrossRefGoogle Scholar
Ross, C. S. and Hendricks, S. B. (1945) Minerals of the montmorillonite group, their origin and relation to soils and clays: U.S. Geol. Survey, Prof. Paper 205B, pp. 2379.Google Scholar