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Quantitative Analyses of Precession Diffraction Data for a Large Cell Oxide

  • Christopher S. Own (a1), Arun K. Subramanian (a1) and Laurence D. Marks (a1)

Kinematical and two-beam calculations have been conducted and are compared to experimental precession data for the large unit cell crystal La4Cu3MoO12. Precession electron diffraction intensities are found to exhibit approximate two-beam behavior and demonstrate clear advantages over conventional SADP intensities for use in structure solution.

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Berg, B.S., Hansen, V., Midgley, P.A., & Gjønnes, J. (1998). Measurement of three-dimensional intensity data in electron diffraction by the precession technique. Ultramicroscopy74, 147157.

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Vander Griend, D.A., Boudin, S., Caignaert, V., Poeppelmeier, K.R., Wang, Y.G., Dravid, V.P., Azuma, M., Takano, M., Hu, Z.B., & Jorgensen, J.D. (1999). La4Cu3MoO12: A novel cuprate with unusual magnetism. J Am Chem Soc121, 4787.

Vincent, R. & Bird, D.M. (1986). Measurement of kinematic intensities from large-angle electron-diffraction patterns. Phil Mag Lett53, L35L40.

Vincent, R. & Midgley, P.A. (1994). Double conical beam-rocking system for measurement of integrated electron-diffraction intensities. Ultramicroscopy53, 271282.

Xu, P., Jayaram, G., & Marks, L.D. (1994). Cross-correlation method for intensity measurement of transmission. Ultramicroscopy53, 1518.

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Microscopy and Microanalysis
  • ISSN: 1431-9276
  • EISSN: 1435-8115
  • URL: /core/journals/microscopy-and-microanalysis
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