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Stability Performance of an Energy Filtering TEM

Published online by Cambridge University Press:  02 July 2020

G. Benner
Affiliation:
LEO Elektronenmikroskopie GmbH, Carl Zeiss Str. 56, 73447, Oberkochen, Germany
E. Zellmann
Affiliation:
LEO Elektronenmikroskopie GmbH, Carl Zeiss Str. 56, 73447, Oberkochen, Germany
A. Harscher
Affiliation:
Inst. Für Angewandte Physik der Universitat Tübingen, Auf der Morgenstelle 12, 72076, Tubingen; Germany
R. Härle
Affiliation:
LEO Elektronenmikroskopie GmbH, Carl Zeiss Str. 56, 73447, Oberkochen, Germany
B. Kabius
Affiliation:
LEO Elektronenmikroskopie GmbH, Carl Zeiss Str. 56, 73447, Oberkochen, Germany
Volker Seybold
Affiliation:
LEO Elektronenmikroskopie GmbH, Carl Zeiss Str. 56, 73447, Oberkochen, Germany
W. Probst
Affiliation:
LEO Elektronenmikroskopie GmbH, Carl Zeiss Str. 56, 73447, Oberkochen, Germany
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Extract

The electron-optical design and the technical realisation of correctors, monochromators and imaging spectrometers as well as methods of resolution improvement (Focus variation, Holography) have made significant progress in the past few years. For all such devices and methods the mechanical and electrical stability of the microscope are the main challenges.

Such requirements are even more critical in case of Energy Filtering Transmission Electron Microscopes (EFTEMs), where the achievement of highly resolved analytical results requires long detection times (in the range of a few 10s of seconds). Resolution in such case could mean both spatial and energy resolution even at the same time. The stability performance of the combined system is more complex than the sum of the stabilities of the single components. Thus, a specified HT short- and long-term stability of 2 ppm is not sufficient to achieve an energy resolution of 0.2 eV at 100 kV acceleration voltage.

Type
Electron Energy-Loss Spectroscopy (EELS) and Imaging
Copyright
Copyright © Microscopy Society of America

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References

[1]Harscher, A.. Lichte, H., Mayer, J.. Ultramicroscopy. 69 (1997) 201209CrossRefGoogle Scholar