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Strain Analysis of Si by FEM and Energy-Filtering CBED

Published online by Cambridge University Press:  28 March 2002

Tetsuya Okuyama
Affiliation:
Department of Materials Science and Engineering, Kurume National College of Technology, Kurume 830-8555, Japan
Masaru Nakayama
Affiliation:
Department of Materials Science and Engineering, Kurume National College of Technology, Kurume 830-8555, Japan
Yoshitsugu Tomokiyo
Affiliation:
Department of Materials Science and Engineering, Kyushu University, Fukuoka 812-8581, Japan
Omer Van der Biest
Affiliation:
Departement Metaalkunde en Toegepaste Materiaalkunde (MTM), Katholieke Universiteit Leuven, de Croylaan 2, B-3001 Leuven, Belgium
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Abstract

Lattice strains around a platelet oxygen precipitate in Si wafer is studied by energy filtering convergent-beam electron diffraction (CBED) and calculations based on the finite element method (FEM). Local lattice strains are measured from CBED patterns obtained with a probe size less than 2 nm in a specimen thicker than 450 nm. Strains measured are compressive along a direction normal to a plate of the precipitate and tensile along a direction parallel to the plate. Two-dimensional stress fields near the precipitate are obtained with FEM computer analyses by fitting the measured strains. It appears that shear stresses are concentrated at the end of the precipitate edge and the maximum shear stress at an interface between the precipitate and the Si-matrix is 1.9 GPa. It is demonstrated that a combination of the energy filtering CBED and FEM is very useful for the study of local strains near interfaces in semiconductor devices, in particular for the study of stress fields that are too steep for application of the conventional CBED technique.

Type
Research Article
Copyright
© 2002 Microscopy Society of America

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