Hostname: page-component-848d4c4894-pftt2 Total loading time: 0 Render date: 2024-05-12T08:24:39.375Z Has data issue: false hasContentIssue false

Structural and Magnetic Properties of Co50 ± x Pt50 ± x Thin Films Prepared by Mbe Co-Evaporation on (001) MgO Substrate at Various Temperatures

Published online by Cambridge University Press:  10 February 2011

V. Parasote
Affiliation:
IPCMS-GEMM, CNRS-ULP, 23 Rue du Loess, F-67037 Strasbourg, France
M.-C. Cadevwlle
Affiliation:
IPCMS-GEMM, CNRS-ULP, 23 Rue du Loess, F-67037 Strasbourg, France
V. Pierron-Bohnes
Affiliation:
IPCMS-GEMM, CNRS-ULP, 23 Rue du Loess, F-67037 Strasbourg, France
W. Grange
Affiliation:
IPCMS-GEMM, CNRS-ULP, 23 Rue du Loess, F-67037 Strasbourg, France
Get access

Abstract

Structural and magnetic properties of Co50 ± x Pt50± x films 25-50 nm thick, prepared by molecular beam epitaxy onto a Pt buffer grown on MgO (001) substrate have been investigated. A series of 3 samples with different compositions (x = 6, 0, -6) was grown at 800 K on a 10 nm thick Pt buffer and another series of 5 samples of equiatomic composition was prepared at various growth temperatures (390 K≤ TG≤ 780 K) on a Pt buffer 4 nm thick. X-ray diffraction and TEM studies show the presence of grains with [111] and [002] orientations, the [002] grains being a mixture of the tetragonal L10 ordered phase and of the fcc disordered one. Both the thickness of the buffer layer and the deposition temperature are determinant parameters of the structural quality of the films and of the degree of long range order (LRO). An apparent LRO parameter (ηapp) is deduced from the superstructure and main peak intensity ratio. Its increase with the growth temperature is described through a thermally activated model that yields a small activation energy of 0.28 eV, illustrating the role played by both surface diffusion and surface interactions in building the L10 compound in agreement with theoretical predictions. An average uniaxial magnetocrystalline anisotropy energy (Kuav) is deduced from the magnetization curves measured by a SQUID. The anisotropy energy of the [002] grains (Ku002) is deduced, assuming a linear relationship between the anisotropies and the phase percentages. One observes a continuous but not linear increase of Ku002 with ηapp.

Type
Research Article
Copyright
Copyright © Materials Research Society 1998

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Eurin, P. and Paulevé, J., IEEE Trans. on Magnetics Mag. 5, 216 (1969).Google Scholar
2. Lairson, B. M. et al. , J. Appl. Phys. 74 (3) 1922 (1993).Google Scholar
3. Visokay, M. R. and Sinclair, R., Appl. Phys. Lett. 66 (13) 1692 (1995).10.1063/1.113895Google Scholar
4. Harp, G. R. et al. , Mat. Res. Soc. Symp. Proc. 313, 493 (1993).10.1557/PROC-313-493Google Scholar
5. Cadeville, M.C. et al. , Physica Scripta, T49 364372 (1993).10.1088/0031-8949/1993/T49A/064Google Scholar
6. Leroux, C. et al. J. Phys. F: Met. Phys. 18, 2033 (1988).10.1088/0305-4608/18/9/021Google Scholar
7. Dahmani, C. E., PhD Thesis Université Louis Pasteur, Strasbourg, France (1985).Google Scholar
8. Cadeville, M. C., Dahmani, C.E. and Kern, F., JMMM 54–57, 1055 (1986).Google Scholar
9. Parasote, V., PhD thesis, Louis Pasteur University, Strasbourg, France (1998).Google Scholar
10. Berg, H. and Cohen, J. B., Metal. Trans., 3, 1797 (1972).10.1007/BF02642563Google Scholar
11. Bouzidi, L. et al. , Thin Solid Films, in press (1998) and Pierron-Bohnes, V. et al. , to be published in “Diffusion Mechanisms in Crystalline Materials” Mat. Res. Soc. Symp. Proc. (1998).Google Scholar
12. Stoeffler, D. and Gautier, F., Surface Science, 249, 265 (1991).Google Scholar
13. Gehanno, V., Marty, A., Gilles, B. and Samson, Y., Phys. Rev. B, 55, 12552 (1997).Google Scholar
14. Dahmani, C.E., Cadeville, M.C. and Pierron-Bohnes, V., Acta Metall., 3, 369 (1985).10.1016/0001-6160(85)90079-3Google Scholar
15. Treglia, G., private communication.Google Scholar
16. Samuka, A., J. Phys. Soc. Jap., 63 3053 (1994).Google Scholar
17. Meneghini, C. et al. , J. Phys. IV France 7 (suppl.), C21115 (1997).Google Scholar