The accuracy and precision of radiocarbon dating largely depend on the quality of sample preparation prior to measurement. Proper selection of material, identification of potential contaminants, and application of appropriate purification procedures are the basis of reliable 14C analyses. Modern preparation laboratories not only support the process of obtaining reliable results but also play a key role in integrating the scientific community and educating future geochronologists. In 2025, a new Laboratory of Preparation for Radiocarbon Dating (LBC14) was established at Maria Curie-Skłodowska University in Lublin, Poland. The laboratory has been adapted for the selection and purification of macroscopic organic samples, such as charcoal, wood, peat, organic sediments, macrofossils, and bone—both unburned and cremated. The protocols used are acid-base-acid (ABA), ultrafiltration, and apatite preparation, modified according to the material’s state of preservation. The paper presents the scope of the new laboratory, the procedures used, and the first results of dating performed at the AMS Laboratory at ETH Zurich. The presented initiative is an important step towards the development of 14C research infrastructure in Poland and the construction of sustainable, interdisciplinary standards for working with dating material.