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Design of porous aluminum oxide ceramics using magnetic field-assisted freeze-casting

Published online by Cambridge University Press:  06 August 2020

Said Bakkar ,
Jihyung Lee ,
Nicholas Ku ,
Diana Berman ,
Samir M. Aouadi ,
Raymond E. Brennan  and
Marcus L. Young
Said Bakkar
Affiliation:
Department of Materials Science and Engineering, University of North Texas, Denton, Texas76203, USA
Jihyung Lee
Affiliation:
Department of Materials Science and Engineering, University of North Texas, Denton, Texas76203, USA
Nicholas Ku
Affiliation:
CIV USARMY CCDC ARL, U.S. Army Research Laboratory, Aberdeen Proving Ground, Maryland21005-5425, USA
Diana Berman
Affiliation:
Department of Materials Science and Engineering, University of North Texas, Denton, Texas76203, USA
Samir M. Aouadi
Affiliation:
Department of Materials Science and Engineering, University of North Texas, Denton, Texas76203, USA
Raymond E. Brennan*
Affiliation:
CIV USARMY CCDC ARL, U.S. Army Research Laboratory, Aberdeen Proving Ground, Maryland21005-5425, USA
Marcus L. Young*
Affiliation:
Department of Materials Science and Engineering, University of North Texas, Denton, Texas76203, USA
*
a)Address all correspondence to these authors. e-mail: raymond.e.brennan.civ@mail.mil
b)e-mail: marcus.young@unt.edu
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Abstract

Magnetic field-assisted freeze-casting of porous alumina structures is reported. Different freeze-casting parameters were investigated and include the composition of the original slurry (Fe3O4 and PVA content) and the control of temperature during the free casting process. The optimum content of the additives in the slurry were 3 and 6 wt% for PVA and Fe3O4, respectively. These conditions provided the most unidirectional porous structures throughout the length of the sample. The sintering temperature was maintained at 1500 °C for 3 h. The application of a vertical magnetic field (parallel to ice growth direction) with using a cooling rate mode technique was found to enhance the homogeneity of the porous structure across the sample. The current study suggests that magnetic field-assisted freeze-casting is a viable method to create highly anisotropic porous ceramic structures.

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Article
Information
Journal of Materials Research , Volume 35 , Issue 21 , 16 November 2020 , pp. 2859 - 2869
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Copyright
Copyright © The Author(s), 2020, published on behalf of Materials Research Society by Cambridge University Press

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References

Hammel, E.C., Ighodaro, O.L.R., and Okoli, O.I.: Processing and properties of advanced porous ceramics: An application based review. Ceram. Int. 40, 15351 (2014).CrossRefGoogle Scholar
Li, D. and Li, M.: Porous Y2SiO5 ceramic with low thermal conductivity. J. Mater. Sci. Technol. 28, 799 (2012).CrossRefGoogle Scholar
Sobsey, M.D., Stauber, C.E., Casanova, L.M., Brown, J.M., and Elliott, M.A.: Response to comment on “Point of use household drinking water filtration: A practical, effective solution for providing sustained access to safe drinking water in the developing world.” Environ. Sci. Technol. 43, 970 (2009).CrossRefGoogle Scholar
Sundaram, S., Colombo, P., and Katoh, Y.: Selected emerging opportunities for ceramics in energy, environment, and transportation. Int. J. Appl. Ceram. Technol. 10, 731 (2013).CrossRefGoogle Scholar
Zhou, M., Shu, D., Li, K., Zhang, W.Y., Ni, H.J., Sun, B.D., and Wang, J.: Deep filtration of molten aluminum using ceramic foam filters and ceramic particles with active coatings. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 34A, 1183 (2003).CrossRefGoogle Scholar
Moene, R., Makkee, M., and Moulijn, J.: High surface area silicon carbide as catalyst support characterization and stability. Appl. Catal. A Gen. 167, 321 (1998).CrossRefGoogle Scholar
Gaudillere, C., Garcia-Fayos, J., Balaguer, M., and Serra, J.M.: Enhanced oxygen separation through robust freeze-cast bilayered dual-phase membranes. ChemSusChem 7, 2554 (2014).CrossRefGoogle ScholarPubMed
Gibson, L.J. and Editor, G.: Cellular Solids. No. April 2003, 270 (2018)CrossRefGoogle Scholar
Deville, S.: Freeze-casting of porous biomaterials: Structure, properties and opportunities. Materials 3, 1913 (2010).CrossRefGoogle Scholar
Deville, S., Saiz, E., and Tomsia, A.P.: Freeze casting of hydroxyapatite scaffolds for bone tissue engineering. Biomaterials 27, 5480 (2006).CrossRefGoogle ScholarPubMed
Soltani, N., Martínez-Bautista, R., Bahrami, A., Huerta Arcos, L., Cassir, M., and Chávez Carvayar, J.: Fabrication of aligned porous LaNi0.6Fe0.4O3 perovskite by water based freeze casting. Chem. Phys. Lett. 700, 138 (2018).CrossRefGoogle Scholar
Bahrami, A., Simon, U., Soltani, N., Zavareh, S., Schmidt, J., Pech-Canul, M.I., and Gurlo, A.: Eco-fabrication of hierarchical porous silica monoliths by ice-templating of rice husk ash. Green Chem. 19, 188 (2017).CrossRefGoogle Scholar
Herzog, A., Klingner, R., Vogt, U., and Graule, T.: Wood-derived porous SiC ceramics by sol infiltration and carbothermal reduction. J. Am. Ceram. Soc. 87, 784 (2004).CrossRefGoogle Scholar
Saboori, A., Rabiee, M., Moztarzadeh, F., Sheikhi, M., Tahriri, M., and Karimi, M.: Synthesis, characterization and in vitro bioactivity of sol-gel-derived SiO2–CaO–P2O5–MgO bioglass. Mater. Sci. Eng. C 29, 335 (2009).CrossRefGoogle Scholar
Studart, A.R., Gonzenbach, U.T., Tervoort, E., and Gauckler, L.J.: Processing routes to macroporous ceramics: A review. J. Am. Ceram. Soc. 89, 1771 (2006).CrossRefGoogle Scholar
Scotti, K.L. and Dunand, D.C.: Freeze casting—A review of processing, microstructure and properties via the open data repository, FreezeCasting.net. Prog. Mater. Sci. 94, 243 (2018).CrossRefGoogle Scholar
Araki, K. and Halloran, J.W.: Porous ceramic bodies with interconnected pore channels by a novel freeze casting technique. J. Am. Ceram. Soc. 88, 1108 (2005).CrossRefGoogle Scholar
Stolze, C., Janoschka, T., Schubert, U.S., Müller, F.A., and Flauder, S.: Directional solidification with constant ice front velocity in the ice-templating process. Adv. Eng. Mater. 18, 111 (2016).CrossRefGoogle Scholar
Arai, N. and Faber, K.T.: Hierarchical porous ceramics via two-stage freeze casting of preceramic polymers. Scr. Mater. 162, 72 (2019).CrossRefGoogle Scholar
Christiansen, C.D., Nielsen, K.K., and Bjørk, R.: Novel freeze-casting device with high precision thermoelectric temperature control for dynamic freezing conditions. Rev. Sci. Instrum. 91, 033904 (2020).CrossRefGoogle ScholarPubMed
Deville, S., Saiz, E., and Tomsia, A.P.: Ice-templated porous alumina structures. Acta Mater. 55, 1965 (2007).CrossRefGoogle Scholar
Li, W.L., Lu, K., and Walz, J.Y.: Freeze casting of porous materials: Review of critical factors in microstructure evolution. Int. Mater. Rev. 57, 37 (2012).CrossRefGoogle Scholar
Nelson, I. and Naleway, S.E.: Intrinsic and extrinsic control of freeze casting. J. Mater. Res. Technol. 8, 2372 (2019).CrossRefGoogle Scholar
Deville, S., Saiz, E., Nalla, R.K., and Tomsia, A.P.: Freezing as a path to build complex composites. Science 311, 515 (2006).CrossRefGoogle ScholarPubMed
Deville, S., Maire, E., Lasalle, A., Bogner, A., Gauthier, C., Leloup, J., and Guizard, C.: In situ X-ray radiography and tomography observations of the solidification of aqueous alumina particle suspensions—Part I: Initial instants. J. Am. Ceram. Soc. 92, 2489 (2009).CrossRefGoogle Scholar
Fukasawa, T., Deng, Z.Y., Ando, M., Ohji, T., and Goto, Y.: Pore structure of porous ceramics synthesized from water-based slurry by freeze-dry process. J. Mater. Sci. 36, 2523 (2001).CrossRefGoogle Scholar
Niksiar, P., Su, F., Frank, M., Ogden, T., Naleway, S., Meyers, M., McKittrick, J., and Porter, M.: External field assisted freeze casting. Ceramics 2, 208 (2019).CrossRefGoogle Scholar
Porter, M.M., Niksiar, P., and McKittrick, J.: Microstructural control of colloidal-based ceramics by directional solidification under weak magnetic fields. J. Am. Ceram. Soc. 99, 1917 (2016).CrossRefGoogle Scholar
Porter, M.M., Yeh, M., Strawson, J., Goehring, T., Lujan, S., Siripasopsotorn, P., Meyers, M.A., and McKittrick, J.: Magnetic freeze casting inspired by nature. Mater. Sci. Eng. A 556, 741 (2012).CrossRefGoogle Scholar
Frank, M.B., Naleway, S.E., Haroush, T., Liu, C.H., Siu, S.H., Ng, J., Torres, I., Ismail, A., Karandikar, K., Porter, M.M., Graeve, O.A., and McKittrick, J.: Stiff, porous scaffolds from magnetized alumina particles aligned by magnetic freeze casting. Mater. Sci. Eng. C 77, 484 (2017).Google ScholarPubMed
Nelson, I., Ogden, T.A., Al Khateeb, S., Graser, J., Sparks, T.D., Abbott, J.J., and Naleway, S.E.: Freeze-casting of surface-magnetized iron(II,III) oxide particles in a uniform static magnetic field generated by a Helmholtz coil. Adv. Eng. Mater. 21, 1 (2019).CrossRefGoogle Scholar
Tang, Y., Qiu, S., Miao, Q., and Wu, C.: Fabrication of lamellar porous alumina with axisymmetric structure by directional solidification with applied electric and magnetic fields. J. Eur. Ceram. Soc. 36, 1233 (2016).CrossRefGoogle Scholar
Zuo, K.H., Zeng, Y.P., and Jiang, D.: Properties of microstructure-controllable porous yttria-stabilized ziroconia ceramics fabricated by freeze casting. Int. J. Appl. Ceram. Technol. 5, 198 (2008).CrossRefGoogle Scholar
Peko, C., Groth, B., and Nettleship, I.: The effect of polyvinyl alcohol on the microstructure and permeability of freeze-cast alumina. J. Am. Ceram. Soc. 93, 115 (2010).CrossRefGoogle Scholar