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Nature of contact deformation of TiN films on steel

  • S. Bhowmick (a1), Z-H. Xie (a2), M. Hoffman (a2), V. Jayaram (a1) and S.K. Biswas (a3)...

Nanoindentation experiments were carried out on a columnar ∼1.5-μm-thick TiN film on steel using a conical indenter with a 5-μm tip radius. Microstructural examination of the contact zone indicates that after initial elastic deformation, the deformation mechanism of the TiN is dominated by shear fracture at inter-columnar grain boundaries of the TiN film. A simple model is proposed whereby the applied load is partitioned between a deforming TiN annulus and a central expanding cavity in the steel substrate. It is possible to obtain a good fit to the experimental load–displacement curves with only one adjustable parameter, namely the inter-columnar shear fracture stress of the TiN film. The implication of results in the context of the performance of TiN films in service is also discussed.

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Journal of Materials Research
  • ISSN: 0884-2914
  • EISSN: 2044-5326
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