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Analysis of Refractory Materials by Energy Dispersive X-Ray Spectrometry

Published online by Cambridge University Press:  06 March 2019

Jim Parker  and
Wayne Watson
Jim Parker
Affiliation:
Manville Research and Development Center P. O. Box 5108 Denver, Colorado 80217
Wayne Watson
Affiliation:
Tracor Xray, Inc. 345 East Middlefield Road Mountainview, California 94043
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Extract

Silica-alumina refractory materials are used as insulation materials in high temperature applications. Such materials are amenable to x-ray analysis (1). Wavelength dispersive x-ray spectrometry is used in our laboratory for the analysis of a variety of refractory materials. An analysis procedure was needed for a quality control project that would provide major and minor element determinations in silica-alumina refractory materials. The requirements for the analysis scheme were relative accuracy and precision to be better than one percent. The method had to be rapid, simple to use, and inexpensive. Energy dispersive x-ray spectrometry and a borate fusion technique were chosen as the method of choice for this application. Described in this paper are the sample and standard preparation procedures, data reduction methods, and analytical results.

Type
Research Article
Information
Advances in X-Ray Analysis , Volume 29: Thirty-Fourth Annual Conference on Applications of X-ray Analysis, August 5-9, 1985 , 1985 , pp. 557 - 564
Copyright
Copyright © International Centre for Diffraction Data 1985

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References

1) Ashley, D.G. and Andrews, K.W., “ Analysis of Aluminosilicate Materials by X- ray Fluorescence Spectrometry”, Analyst. 97 :841 (1972).Google Scholar
2) Bowling, G.D., Ailin- Pyzik, I.B., and Jones, D.R. IV. “A Rapid, Lew Cost, Manual Fusion Sample Preparation Technique for Quantitative X- ray Fluorescence Analysis “, Advances in X- ray Analysis. Vol. 27, p. 491 (1984).Google Scholar
3) Bennett, H. and Oliver, G.J., “Development of Fluxesforttie Analysis of Ceramic Materials by X-ray Fluorescence Spectrometry”, Analyst. 101: 803 (1976).Google Scholar
4) Sastry, B.S.R. and Hummel, F.A., “Studies in Lithium Oxide Systems: I. Li2O.B202-B203“l, Journal of the American Ceramic Society. 41 :7 (1958).Google Scholar