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Instrumentation for structure measurements on highly non-equilibrium materials

Published online by Cambridge University Press:  22 February 2011

J. K. R. Weber ,
C. J. Benmore ,
M. C. Wilding ,
J. Neuefeind  and
J. B. Parise
J. K. R. Weber*
Affiliation:
Materials Development, Inc., 3090 Daniels Court, Arlington Heights, IL 60004, USA Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, IL 60439, USA
C. J. Benmore
Affiliation:
Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, IL 60439, USA
M. C. Wilding
Affiliation:
Institute of Mathematics and Physics, Aberystwyth University, Aberystwyth, SY23 3BZ, UK
J. Neuefeind
Affiliation:
Spallation Neutron Source, Oak Ridge National Laboratory, 1 Bethel Valley Road, Oak Ridge, TN 37830, USA
J. B. Parise
Affiliation:
Department of Geosciences and Department of Chemistry, Stony Brook University, Stony Brook, NY 11794, USA
*
†Email address for correspondence:rweber@anl.gov
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Abstract

Containerless techniques (levitation) completely eliminate contact with the sample. This unique sample environment allows deep supercooling of many liquids and avoids contamination of high-temperature melts. Recent experiments at the Advanced Photon Source (APS) high-energy beamline 11 ID-C used aerodynamic levitation with laser beam heating and acoustic levitation with cryogenic cooling. By using these two methods, liquids were studied over much of the temperature range from −40 to +2500°C. This paper briefly describes the instrumentation and its use and is illustrated with examples of measurements on molten oxides and low-temperature liquids.

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Type
Contributed paper
Information
Diamond Light Source Proceedings , Volume 1 , Issue SRMS-7 , October 2010 , e134
Copyright
Copyright © Diamond Light Source Ltd 2011

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References

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