Skip to main content
×
Home
    • Aa
    • Aa
  • Get access
    Check if you have access via personal or institutional login
  • Cited by 45
  • Cited by
    This article has been cited by the following publications. This list is generated based on data provided by CrossRef.

    Camposilvan, Erik and Anglada, Marc 2016. Size and plasticity effects in zirconia micropillars compression. Acta Materialia, Vol. 103, p. 882.


    Dingreville, Rémi Karnesky, Richard A. Puel, Guillaume and Schmitt, Jean-Hubert 2016. Review of the synergies between computational modeling and experimental characterization of materials across length scales. Journal of Materials Science, Vol. 51, Issue. 3, p. 1178.


    Hu, T. Ma, K. Topping, T.D. Jiang, L. Zhang, D. Mukherjee, A.K. Schoenung, J.M. and Lavernia, E.J. 2016. Disordered dislocation configuration in submicrometer Al crystal subjected to plane strain bending. Scripta Materialia, Vol. 113, p. 35.


    Pandey, A. Wheeler, R. Shyam, A. and Stoughton, T. B. 2016. Onset of Plasticity via Relaxation Analysis (OPRA). Experimental Mechanics, Vol. 56, Issue. 6, p. 1095.


    Ramachandramoorthy, Rajaprakash Gao, Wei Bernal, Rodrigo and Espinosa, Horacio 2016. High Strain Rate Tensile Testing of Silver Nanowires: Rate-Dependent Brittle-to-Ductile Transition. Nano Letters, Vol. 16, Issue. 1, p. 255.


    Rudolf, Chris Boesl, Benjamin and Agarwal, Arvind 2016. In Situ Mechanical Testing Techniques for Real-Time Materials Deformation Characterization. JOM, Vol. 68, Issue. 1, p. 136.


    Wang, Jiangwei and Mao, Scott X. 2016. Atomistic perspective on in situ nanomechanics. Extreme Mechanics Letters,


    Bernal, Rodrigo A. Ramachandramoorthy, Rajaprakash and Espinosa, Horacio D. 2015. Double-tilt in situ TEM holder with multiple electrical contacts and its application in MEMS-based mechanical testing of nanomaterials. Ultramicroscopy, Vol. 156, p. 23.


    Camposilvan, Erik and Anglada, Marc 2015. Micropillar compression inside zirconia degraded layer. Journal of the European Ceramic Society, Vol. 35, Issue. 14, p. 4051.


    Deng, Chuang and Sansoz, Frederic 2015. A new form of pseudo-elasticity in small-scale nanotwinned gold. Extreme Mechanics Letters,


    Kuan, S.Y. Huang, J.C. Chen, Y.H. Chang, C.H. Hsieh, C.H. Wang, J.H. Nian, Y.C. Ju, S.P. Nieh, T.G. Chen, S.H. and Hwang, Y.M. 2015. Extended elastic region in nanocrystalline HCP and FCC metals under nano-tension loading. Materials Science and Engineering: A, Vol. 646, p. 135.


    Romeis, Stefan Paul, Jonas Herre, Patrick Hanisch, Mathias Taylor, Robin N. Klupp Schmidt, Jochen and Peukert, Wolfgang 2015. In Situ Deformation and Breakage of Silica Particles Inside a SEM. Procedia Engineering, Vol. 102, p. 201.


    Sarkar, Rohit Rentenberger, Christian and Rajagopalan, Jagannathan 2015. Electron Beam Induced Artifacts During in situ TEM Deformation of Nanostructured Metals. Scientific Reports, Vol. 5, p. 16345.


    Wheeler, R. Pandey, A. Shyam, A. Tan, T. and Lara-Curzio, E. 2015. Small Scale Mechanical Characterization of Thin Foil Materials via Pin Load Microtesting. Experimental Mechanics, Vol. 55, Issue. 7, p. 1375.


    Bergers, L I J C Hoefnagels, J P M and Geers, M G D 2014. On-wafer time-dependent high reproducibility nano-force tensile testing. Journal of Physics D: Applied Physics, Vol. 47, Issue. 49, p. 495306.


    Bernal, Rodrigo A. Filleter, Tobin Connell, Justin G. Sohn, Kwonnam Huang, Jiaxing Lauhon, Lincoln J. and Espinosa, Horacio D. 2014. In Situ Electron Microscopy Four-Point Electromechanical Characterization of Freestanding Metallic and Semiconducting Nanowires. Small, Vol. 10, Issue. 4, p. 725.


    Bhattacharyya, Dhriti Wheeler, Robert W. Harrison, Robert P. and Edwards, Lyndon 2014. The Observation of Slip Phenomena in Single Crystal Fe Samples During In Situ Micro-Mechanical Testing Through Orientation Imaging. Microscopy and Microanalysis, Vol. 20, Issue. 04, p. 1060.


    Camposilvan, Erik Torrents, Oscar and Anglada, Marc 2014. Small-scale mechanical behavior of zirconia. Acta Materialia, Vol. 80, p. 239.


    Hÿtch, Martin J. and Minor, Andrew M. 2014. Observing and measuring strain in nanostructures and devices with transmission electron microscopy. MRS Bulletin, Vol. 39, Issue. 02, p. 138.


    McLean, M. J. Wade, C. A. Watanabe, M. and Vinci, R. P. 2014. Microscale Fracture Toughness of Bismuth Doped Copper Bicrystals Using Double Edge Notched Microtensile Tests. Experimental Mechanics, Vol. 54, Issue. 4, p. 685.


    ×

Quantitative In Situ Mechanical Testing in Electron Microscopes

Abstract
Abstract

This article is devoted to recent progress in the area of in situ electron microscopy (scanning and transmission) and will focus on quantitative aspects of these techniques as applied to the deformation of materials. Selected recent experiments are chosen to illustrate how these techniques have benefited from improvements ranging from sample preparation to digital image acquisition. Known for its ability to capture the underlying phenomena of plastic deformation as they occur, in situ electron microscopy has evolved to a level where fully instrumented micro- and nanomechanical tests can be performed simultaneously.

Copyright
Linked references
Hide All

This list contains references from the content that can be linked to their source. For a full set of references and notes please see the PDF or HTML where available.

1.Z. Budrovic , H. Van Swygenhoven , P.M. Derlet , S. Van Petegem , B. Schmitt , Science 304 (5668), 273 (2004).

2.R. Maass , S. Van Petegem , D. Grolimund , H. Van Swygenhoven , D. Kiener , G. Dehm , Appl. Phys. Lett. 92 (7), 071905 (2008).

3.J.S. Kim , T. LaGrange , B.W. Reed , M.L. Taheri , M.R. Armstrong , W.E. King , N.D. Browning , G.H. Campbell , Science 321 (5895), 1472 (2008).

4.D. Shorokhov , A.H. Zewail , Phys. Chem. Chem. Phys. 10 (20), 2879 (2008).

5.J.K. Deuschle , G. Buerki , H.M. Deuschle , S. Enders , J. Michler , E. Arzt , Acta Mater. 56 (16), 4390 (2008).

7.N. Gane , F.P. Bowden , J. Appl. Phys. 39 (3), 1432 (1968).

8.N. Gane , Proc. R. Soc. London, Ser. A 317 (1530), 367 (1970).

10.N.A. Fleck , G.M. Muller , M.F. Ashby , J.W. Hutchinson , Acta Mater. 42, 475 (1994).

11.J.S. Stolken , A.G. Evans , Acta Mater. 46, 5109 (1998).

12.M.A. Haque , M.T.A. Saif , Acta Mater. 51, 3053 (2003).

13.C. Motz , T. Schöberl , R. Pippan , Acta Mater. 53 (15), 4269 (2005).

14.S. Wurster , C. Motz , M. Jenko , R. Pippan , Adv. Eng. Mater. 12, 61 (2009).

15.J. Silcox , M.J. Whelan , Philos. Mag. 5, 1 (1960).

16.F. Louchet , L.P. Kubin , D. Vesely , Philos. Mag. A. 39 (4), 433 (1979).

17.A. Couret , J. Crestou , S. Farenc , G. Molenat , N. Clément , A. Coujou , D. Caillard , Microsc. Microanal. Microstruct. 4, 153 (1993).

18.A. Jacques , A. George , M. Polcarova , J. Bradler , Nucl. Instrum. Methods Phys. Res., Sect. B 200, 261 (2003).

19.G. Vanderschaeve , D. Caillard , Mater. Sci. Eng., A 462 (1–2), 418 (2007).

20.F. Mompiou , D. Caillard , M. Feuerbacher , Philos. Mag. A. 84 (25–26), 2777 (2004).

21.M. Legros , A. Couret , D. Caillard , Philos. Mag. A 73 (1), 81 (1996).

22.M. Legros , Y. Minonishi , D. Caillard , Philos. Mag. A 76 (5), 1013 (1997).

23.M. Legros , N. Clement , P. Caron , A. Coujou , Mater. Sci. Eng., A 337 (1–2), 160 (2002).

24.S. Farenc , A. Coujou , A. Couret , Philos. Mag. 67 (11), 127 (1993).

25.S.H. Oh , M. Legros , D. Kiener , P. Gruber , G. Dehm , Acta Mater. 55 (16), 5558 (2007).

26.M. Legros , D.S. Gianola , K.J. Hemker , Acta Mater. 56, 3380 (2008).

27.D. Caillard , Philos. Mag. Lett. 89 (8), 517 (2009).

29.M.D. Uchic , D.M. Dimiduk , J.N. Florando , W.D. Nix , Science 305 (5686), 986 (2004).

30.J.R. Greer , C.R. Weinberger , W. Cai , Mater. Sci. Eng., A 493 (1–2), 21 (2008).

31.J. Greer , J.-Y. Kim , M. Burek , JOM 61 (12), 19 (2009).

32.D. Kiener , W. Grosinger , G. Dehm , R. Pippan , Acta Mater. 56 (3), 580 (2008).

33.Z.W. Shan , R.K. Mishra , S.A.S. Asif , O.L. Warren , A.M. Minor , Nat. Mater. 7 (2), 115 (2008).

34.H. Bei , S. Shim , M.K. Miller , G.M. Pharr , E.P. George , Appl. Phys. Lett. 91 (11), 111915 (2007).

35.S. Shim , H. Bei , M.K. Miller , G.M. Pharr , E.P. George , Acta Mater. 57 (2), 503 (2009).

36.H. Bei , S. Shim , E.P. George , M.K. Miller , E.G. Herbert , G.M. Pharr , Scr. Mater. 57 (5), 397 (2007).

37.D. Zhang , J.-M. Breguet , R. Clavel , L. Phillippe , I. Utke , J. Michler , Nanotechnology 20, 36 (2009).

38.F. Östlund , K. Rzepiejewska-Malyska , K. Leifer , L.M. Hale , Y. Tang , R. Ballarini , W.W. Gerberich , J. Michler , Adv. Funct. Mater. 19 (15), 2439 (2009).

39.M. Legros , M. Cabié , D.S. Gianola , Microsc. Res. Tech. 72 (3), 270 (2009).

40.M. Jin , A.M. Minor , E.A. Stach , J.J.W. Morris , Acta Mater. 52 (18), 5381 (2004).

41.J.H. Han , M.T.A. Saif , Rev. Sci. Instrum. 77, 4 (2006).

43.J. Rajagopalan , J.H. Han , M.T.A. Saif , Science 315, 1831 (March 2007).

44.J. Rajagopalan , J.H. Han , M.T.A. Saif , Scr. Mater. 59, 734 (2008).

45.M. Legros , K.J. Hemker , A. Gouldstone , S. Suresh , R.M. Keller-Flaig , E. Arzt , Acta Mater. 50 (13), 3435 (2002).

47.Y. Zhu , A. Corigliano , H.D. Espinosa , J. Micromech. Microeng. 16, 242 (2006).

48.A.M. Minor , S.A.S. Asif , Z.W. Shan , E.A. Stach , E. Cyrankowski , T.J. Wyrobek , O.L. Warren , Nat. Mater. 5 (9), 697 (2006).

50.T.C. Chu , W.F. Ranson , M.A. Sutton , W.H. Peters , Exp. Mech. 25 (3), 232 (1985).

51.M.A. Sutton , N. Li , D.C. Joy , A.P. Reynolds , X. Li , Exp. Mech. 47 (6), 775 (2007).

52.D. Caillard , F. Mompiou , M. Legros , Acta Mater. 57 (8), 2390 (2009).

53.F. Mompiou , D. Caillard , M. Legros , Acta Mater. 57 (7), 2198 (2009).

55.M.J. Hÿtch , F. Houdellier , F. Hüe , E. Snoeck , Nature 453, 1086 (2008).

56.M. Uchic , P. Shade , D. Dimiduk , JOM 61 (3), 36 (2009).

57.S.S. Brenner , J. Appl. Phys. 27 (12), 1484 (1956).

58.H. Bei , Y.F. Gao , S. Shim , E.P. George , G.M. Pharr , Phys. Rev. B: Condens. Matter 77 (6), 060103 (2008).

59.D.M. Norfleet , D.M. Dimiduk , S.J. Polasik , M.D. Uchic , M.J. Mills , Acta Mater. 56 (13), 2988 (2008).

60.C. Motz , D. Weygand , J. Senger , P. Gumbsch , Acta Mater. 56 (9), 1942 (2008).

61.G. Dehm , M. Legros , B. Heiland , J. Mater. Sci. 41, 4484 (2006).

62.S.H. Oh , M. Legros , D. Kiener , G. Dehm , Nat. Mater. 8, 95 (2009).

63.G. Richter , K. Hillerich , D.S. Gianola , R. Mönig , O. Kraft , C.A. Volkert , Nano Lett. 9 (8), 3048 (2009).

64.S. Ogata , J. Li , N. Hirosaki , Y. Shibutani , S. Yip , Phys. Rev. B: Condens. Matter 70 (10), (2004).

65.S.S. Brenner , J. Appl. Phys. 28 (9), 1023 (1957).

66.J.W. Cahn , J.E. Taylor , Acta Mater. 52 (16), 4887 (2004).

67.J.W. Cahn , Y. Mishin , A. Suzuki , Acta Mater. 54 (19), 4953 (2006).

68.D.S. Gianola , C. Eberl , JOM 61 (3), 24 (2009).

Recommend this journal

Email your librarian or administrator to recommend adding this journal to your organisation's collection.

MRS Bulletin
  • ISSN: 0883-7694
  • EISSN: 1938-1425
  • URL: /core/journals/mrs-bulletin
Please enter your name
Please enter a valid email address
Who would you like to send this to? *
×