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Characterization of Silver Doped Hydroxyapatite Prepared by EDTAChelate Decomposition Method

Published online by Cambridge University Press:  20 January 2012

Kubra Celik ,
Celaletdin Ergun  and
Huseyin Kizil
Kubra Celik
Affiliation:
Materials Science and Engineering, Istanbul Technical University, 34469 Istanbul, Turkey.
Celaletdin Ergun
Affiliation:
Mechanical Engineering, Istanbul Technical University, 34437 Istanbul, Turkey.
Huseyin Kizil
Affiliation:
Materials Science and Engineering, Istanbul Technical University, 34469 Istanbul, Turkey.
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Abstract

In this study, Ag doped hydroxyapatite (HA) samples prepared by EDTA chelatedecomposition method were characterized with X-Ray Diffraction Spectroscopy(XRD), Scanning Electron Microscopy (SEM) and antimicrobial sensitivitytest. Hydroxyapatite (Ca10(PO)6(OH)2) and NaCaPO4 (rhenanite) phases were observed while Ag was presentin the form of Ag2O. Results showed that microstructurallycontrolled HA-based composites with NaCaPO4 interphase can beprepared, which significantly enhances sinterability of hydroxyapatite at1100° C without formation of any undesired second phases, such as tricalciumphosphate (TCP) known to decrease the stability of HA. The antibacterialsensitivity was tested with E.Coli gram-negative bacteria. The radius ofcircle enclosing the sample increases with increasing Ag content in thestructure as an indication of the region of non-bacterial activity.

Keywords

biomaterialAgphase transformation

Information

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 1418: Symposium LL/MM – Gels and Biomedical Materials , 2012 , mrsf11-1418-mm03-24
Copyright
Copyright © Materials Research Society 2012

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References

REFERENCES

1. Anee, T.K., Ashok, M., Palanichamy, M., Kalkura, S. N., Mater. Chem. and Phys. 80, 725–730, (2003).CrossRefGoogle Scholar
2. Raynaud, S., Champion, E., Bernache-Assollant, D., Thomas, P., Biomaterials 23, 1065–1072, (2002).CrossRefGoogle Scholar
3. Shareef, M.Y., Messer, P.F., van Noort, R., Biomaterials 14(1), 69–75, (1993).CrossRefGoogle Scholar
4. Ergun, C., European Ceramic Society 28, 2137–2149, (2008).CrossRefGoogle Scholar
5. Erck, R., Fenske, G., Thin Solid Films 181, 521, (1989).CrossRefGoogle Scholar
6. Liedberg, H., Lundeberg, T., J. Urol. Res. 17, 359, (1989).CrossRefGoogle Scholar
7. Badrour, L., Sadel, A., Zahir, M., Kimakh, L., Hajbi, A. E., Ann Chem. Sci. Mater. 23, 61–64, (1998).CrossRefGoogle Scholar
8. Joosten, U., Joist, A., Gosheger, G., Liljenqvist, U., Brandt, B., Eiff, C.V., Biomaterials 26, 5251–5258, (2005).CrossRefGoogle Scholar
9. Shirkhanzadeh, M., Azadegan, M., Liu, G. Q., Materials Letters 24, 7–12, (1995).CrossRefGoogle Scholar
10. Yusufoglu, Y., Akinci, M., J. Amer. Ceram. Soc., 91(10), 3147–3153, (2008).CrossRefGoogle Scholar
11. Shih, W. J., Chen, Y. F., Wang, M. C., Hon, M. H., J. of Crystal Growth 270, 211–218, (2004).CrossRefGoogle Scholar