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Millimeter-Wave Driven Polyol Processing of Nanocrystalline Metals

Published online by Cambridge University Press:  14 March 2011

L. K. Kurihara ,
D. Lewis ,
A. M. Jung ,
A. W. Fliflet  and
R. W. Bruce
L. K. Kurihara
Affiliation:
Multifunctional Materials Branch, Code 6350 Also at Potomac Research Int., Fairfax, VA Naval Research Laboratory, Washington, DC 20375, Email: kurihara@anvil.nrl.navy.mil
D. Lewis
Affiliation:
Multifunctional Materials Branch, Code 6350 Naval Research Laboratory, Washington, DC 20375, Email: kurihara@anvil.nrl.navy.mil
A. M. Jung
Affiliation:
Beam Physics Branch, Code 6790
A. W. Fliflet
Affiliation:
Beam Physics Branch, Code 6790 Naval Research Laboratory, Washington, DC 20375, Email: kurihara@anvil.nrl.navy.mil
R. W. Bruce
Affiliation:
LET Corp., Washington, DC Naval Research Laboratory, Washington, DC 20375, Email: kurihara@anvil.nrl.navy.mil
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Abstract

Nanocrystalline metallic powders and coatings have been synthesized using a millimeter wave driven polyol process. We have been able to prepare powders of single elements, alloys, metastable alloys, composites and coatings. Examples of a few of the metals processed in this study include Fe, Co, Ni, Cu, Ru, Rh, Pt, Au, FePt, FexCo100−x, NiAg and Cu-Ni. The polyol experiment was set up in the millimeter wave processing chamber, the beam was directed into the center of the solution and it was brought to reflux, using the millimeter wave beam as a heat source. Varying the power input easily controlled the rate of reflux.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 634: Symposium B – Structure and Mechanical Properties of Nanophase Materials-Theory & Computer Simulations vs. Experiment , 2000 , B6.15.1
Copyright
Copyright © Materials Research Society 2001

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References

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