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New Synthetic Pathways to Mesostructured Thiogermanates

Published online by Cambridge University Press:  16 February 2011

N. Oberender
Affiliation:
Institute of Inorganic and Applied Chemistry, University of Hamburg, Martin-Luther-King Platz 6, 20146 Hamburg, Germany, froeba@xray.chemie.uni-hamburg.de
M. Fröba
Affiliation:
Institute of Inorganic and Applied Chemistry, University of Hamburg, Martin-Luther-King Platz 6, 20146 Hamburg, Germany, froeba@xray.chemie.uni-hamburg.de
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Abstract

The synthesis and characterisation of several mesostructured thiogermanates are shown. In particular the first supramolecular templated synthesis of mesostructured binary metal chalcogenides in a microwave is presented. The obtained products are characterised by x-ray powder diffraction, transmission electron microscopy, thermal analysis and x-ray absorption spectroscopy.

Type
Research Article
Copyright
Copyright © Materials Research Society 1999

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References

1. Kresge, C.T., Leonowicz, M.E., Roth, W.J., Vartuli, J.C., Beck, J.S., Nature, 1992, 359, 710 Google Scholar
2. Huo, Q., Margolese, D.I., Ciesla, U., Feng, P., Gier, T.E., Sieger, P., Leon, R., Petroff, P.M., Schiith, F., Stucky, G.D., Nature, 1994, 368, 317 Google Scholar
3. Bedard, R.L., Vail, L.D., Wilson, S.T., Flanigan, E.M., United States Patent, 1989, No. 4,880,761 Google Scholar
4. Anderson, M.T., Newcomer, P., Mat.Res.Soc.Symp.Proc., 1995, 380, 325 Google Scholar
5. Braun, P.V., Osenar, P., Stupp, S.I., Nature, 1996, 371, 117 Google Scholar
6. Li, J.Q., Kessler, H., Delmotte, L., J Chem. Soc., Faraday Trans., 1997, 4, 665 Google Scholar
7. Li, J.Q., Delmotte, L., Kessler, H., J. Chem. Soc., Chem. Commun., 1996, 1023 Google Scholar
8. Li, J.Q., Kessler, H., Microporous Materials, 1997, 9, 141 Google Scholar
9. Li, J.Q., Kessler, H., Soulard, M., Khouchaf, L., Tilier, M.-H., Adv. Mater., 1998, 10, 946.Google Scholar
10. Fröba, M., Oberender, N., Chem. Commun., 1997, 1729 Google Scholar
11. Bonhomme, F., Kanatzidis, M.G., Chem. Mater., 1998, 10, 1153 Google Scholar
12. Krebs, B., Angew. Chem., 1983, 95, 113 Google Scholar
13. Pohl, S., Krebs, B., Z anorg. allg. Chem., 1976, 424, 265 Google Scholar
14. Ressler, T., J Synchrotron Rad, 1998, 5, 118 Google Scholar
15. Rehr, J.J., Mustre de Leon, J., Zabinsky, S.I., Albers, R.C., J. Am. Chem. Soc., 1991, 113, 5135 Google Scholar
16. MacLachlan, M.J., Petrov, S., Bedard, R.L., Manners, I., Ozin, G.A., Angew. Chem., 1998, 110, 2186 Google Scholar