Hostname: page-component-89b8bd64d-b5k59 Total loading time: 0 Render date: 2026-05-08T03:44:35.392Z Has data issue: false hasContentIssue false
  • English
  • Français

X-ray powder diffraction data for schisanhenol

Published online by Cambridge University Press:  10 October 2013

Li Li Zhang ,
Dan Xiao ,
Xia Lin ,
Wei Luo ,
Si Li  and
Hui Li
Li Li Zhang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Dan Xiao
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Xia Lin
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Wei Luo
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Si Li
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a) Author to whom correspondence should be addressed. Electronic mail: lihuilab@sina.com
Get access

Abstract

Experimental X-ray powder diffraction data, unit-cell parameters and space group for schisanhenol, C23H30O6, are reported [a = 14.6157 Å, b = 12.8801 Å, c = 11.4907 Å, unit-cell volume V = 2163.14 Å3, Z = 4, and space group P212121]. All of the measured lines were indexed and are consistent with the P212121 space group. No detectable impurities were observed.

Keywords

X-ray powder diffractionschisanhenolSchisandra chinensisRietveld refinement

Information

Type
New Diffraction Data
Information
Powder Diffraction , Volume 29 , Issue 1 , March 2014 , pp. 48 - 50
Copyright
Copyright © International Centre for Diffraction Data 2013 

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Article purchase

Temporarily unavailable

References

Chen, M., Kilgore, N., Lee, K. H., Chen, D. F. (2006). “Rubrisandrins A and B, lignans and related anti-HIV compounds from Schisandra rubriflora ,” J. Nat. Prod. 69, 1697–1701.CrossRefGoogle Scholar
Engel, G. E., Wilke, S., König, O., Harris, K. D. M. and Leusen, F. J. J. (1999). “Powder Solve – a complete package for crystal structure solution from powder diffraction patterns,” J. Appl. Crystal. 32, 1169–1179.Google Scholar
Liu, J. S., Huang, M. F., Gao, Y. L. (1978). “Studies on the constituents of Yi–Geng–Wu–Zi (Schisandra henr yi clarke)-I The structures of schisanhenol and deoxyschisandrin,” Acta Chim. Sin. 36, 193–197.Google Scholar
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q. and Li, H. (2012). “Comparative crystal structure determination of griseofulvin: Powder X-ray diffraction versus Single-crystal X-ray diffraction,” Chin. Sci. Bull. 57, 3867–3871.Google Scholar
Xu, C. F., Bao, G. H., He, C. H. (1982). “The crystal structure of Schisanhenol,” Kexue Tongbao (in Chinese) 27, 1081–1084.Google Scholar
Xue, J. Y., Liu, G. T., Wei, H. L., Pan, Y. (1992). “Antioxidant activity of two dibenzocyclooctene lignans on the aged and ischemic brain in rats,” Free Radical Biol. Med. 12, 127–135.Google Scholar
Young, R. A. (1993). The Rietveld Method, IUCr Monographies of Crystallography (Wiley, Oxford).Google Scholar
Yu, L. H., Liu, G. T., Sun, Y. M., Zhang, H. Y. (2004). “Antioxidative effect of schisanhenol on human low density lipoprotein and its quantum chemical calculation,” Acta Pharmacol. Sin. 25, 1038–1044.Google Scholar
Supplementary material: File

Zhang Supplementary Material

Table

Download Zhang Supplementary Material(File)
File 15.9 KB