Hostname: page-component-848d4c4894-4hhp2 Total loading time: 0 Render date: 2024-05-19T12:46:13.224Z Has data issue: false hasContentIssue false

Standard Reference Materials for X-Ray Diffraction Part I. Overview of Current and Future Standard Reference Materials

Published online by Cambridge University Press:  10 January 2013

A. L. Dragoo
Affiliation:
Ceramics Div., Institute for Materials Science and Engineering, National Bureau of Standards, Gaithersburg, MD 20899, U.S.A.

Abstract

Standard Reference Materials (SRM) are stable materials which have one or more properties certified by the National Bureau of Standards. A general introduction is given to the types of SRM's and their certification. SRM's for X-ray diffraction are described in detail, including their intended use and their certified and other properties. New SRM's are under consideration as quantitative standards, intensity and line shape standards, and materials properties standards.

Type
Research Article
Copyright
Copyright © Cambridge University Press 1986

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. NBS Standard Reference Materials Catalog 1986–87; NBS Spec. Publ. 260; pp. 3–6. Edited by Seward, R. W.. Natl. Bur. of Stand., Gaithersburg, MD, June 1986.Google Scholar
2.Taylor, J. K., Handbook for SRM Users; NBS Spec. Publ. 260–100. Natl. Bur. Stand., Gaithersburg, MD, Sept. 1985.Google Scholar
3.Hubbard, C. R., “Standard Reference Material 640a, Silicon Powder 2θ/d-Spacing Standard for X-ray Diffraction”; SRM Certificate, Feb. 1982. Natl. Bur. Stand., Gaithersburg, MD 20899.Google Scholar
4.Swanson, H. E., McMurdie, H. F., Morris, M. C., and Evans, E. H., Standard X-Ray Diffraction Powder Patterns; NBS Monograph 25, Section 4, p. 3, 1966. Natl. Bur. Stand., Gaithersburg, MD 20899.Google Scholar
5.Hubbard, C. R., “Certification of Si Powder Diffraction Standard Reference Material 640a,” J. Appl. Cryst. 16, 285–88 (1983).CrossRefGoogle Scholar
6.Evans, H. T. Jr., Appleman, D. E. and Handwerker, D. S., Report PB216188, 1963. US Department of Commerce, Natl. Techn. Infor. Service, 5285 Port Royal Rd., Springfield, VA 22161.Google Scholar
7.Deslattes, R. D. and Henins, A., Phys. Rev. Letters, 31, 972–75 (1973).CrossRefGoogle Scholar
8.Morris, M. C., McMurdie, H. F., Evans, E. H., Paretzkin, B., deGroot, J. H., Hubbard, C. R. and Carmel, S. J., Standard X-Ray Diffraction Powder Patterns; NBS Monograph 25, Section 13, p. 35, 1976. Natl. Bur. Stand., Gaithersburg, MD 20899.CrossRefGoogle Scholar
9.Hubbard, C. R., “Standard Reference Material 675, Low 2θ (Large d-Spacing) Standard for X-Ray Powder Diffraction”; SRM Certificate, Natl. Bur. Stand., June 1982. Gaithersburg, MD 20899.Google Scholar
10.Pyrros, N. P. and Hubbard, C. R., “Rational Functions as Profile Models in Powder Diffraction,” J. Appl. Cryst. 16, 289–94 (1983).CrossRefGoogle Scholar
11.Hubbard, C. R., “Standard Reference Material 674, X-Ray Powder Diffraction Intensity Set”; SRM Certificate, June 1983. Natl. Bur. Stand., Gaidiersburg, MD 20899.Google Scholar
12.McKenzie, R. L. and Hubbard, C. R., “Standard Reference Material 1878, Respirable Alpha Quartz” (Quantitative X-Ray Powder Diffraction Standard); SRM Certificate, Nov. 1983. Natl. Bur. Stand., Gaidiersburg, MD 20899.Google Scholar
13.NIOSH Manual of Analytical Methods, Vol. 5, may be ordered from die Superintendent of Documents, U.S. Government Printing Office, Washington, D.C. 20402; or from the National Technical Information Service, Springfield, VA 22161.Google Scholar
14.Chung, F., J. Appl. Cryst., 6, 225 (1973).CrossRefGoogle Scholar
15.Hicho, G. E. and Pella, P., “Standard Reference Material 488, 21½% Austenite in Ferrite,” SRM Certificate, Oct. 1983. Natl. Bur. Stand., Gaidiersburg, MD 20899.Google Scholar
16.Hicho, G. E. and Eaton, E. E., “Preparation and Certification of Standard Reference Materials to be Used in the Determination of Retained Austenite in Steels,” Adv. X-Ray Analysis, Vol. 26, 137–40. Edited by Hubbard, C. R., Barrett, C. S., Predecki, P. K. and Leydon, D. E.. Plenum: New York (1983).Google Scholar
17.Shives, T. R., Myerson, M. R. and Gerhold, W. F., “Standard Reference Material 493, Spheroidized Iron Carbide (Fe3C) in Ferrite”; SRM Certificate, March 1985. Nat. Bur. Stand., Gaithersburg, MD.Google Scholar
18.Struble, L. and Lenker, S., Workshop on Quantitative X-Ray Diffraction Analysis, June 1986. Natl. Bur. Stand., Gaithersburg, MD 20899. Abstract.Google Scholar