Hostname: page-component-848d4c4894-75dct Total loading time: 0 Render date: 2024-05-19T08:43:45.224Z Has data issue: false hasContentIssue false

Texture Correction in Phase Analysis and Thin Film Studies

Published online by Cambridge University Press:  10 January 2013

V. Valvoda
Affiliation:
Charles University, Prague, Ke Karlovu 5, 121 16 Prague 2, Czechoslovakia

Abstract

A method is presented for correction of integrated X-ray intensities for preferred orientation of crystallites in a spinning specimen. It is based upon direct integration of the data obtainable from pole distribution of a single crystallographic plane. This pole distribution can be determined from measurements on a texture goniometer or, in special cases, from an ω-scan or from intensities of all reflections measured on a powder diffractometer only. The method was tested on four samples of magnesium and magnesium cadmium alloys and applied to hexagonal BN and α-Ti(N) surface layers. The method was developed with regard to application in phase analysis and thin film studies.

Type
Research Article
Copyright
Copyright © Cambridge University Press 1986

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

Bunge, H.-J. (1969). Mathematische Methoden der Texturanalyse. Berlin: Akademie Verlag.Google Scholar
Čapková, P. and Valvoda, V. (1974). Czech. J. Phys. B24, 891900.CrossRefGoogle Scholar
International Tables for X-ray Crystallography, Vol. 2., (1959). Ed. Kasper, J. S. and Lonsdale, K., Birmingham: Kynoch Press, p. 291.Google Scholar
Järvinen, M., Merisalo, M., Pesonen, A. and Inkinen, O. (1970). J. Appl. Cryst. 3, 313318.CrossRefGoogle Scholar
Jetter, L. K., McHargue, C. J. and Williams, R. O. (1956). J. Appl. Phys. 27, 368374.CrossRefGoogle Scholar
Rietveld, H. M. (1969). J. Appl. Cryst. 2, 6571.CrossRefGoogle Scholar
Roe, R. J. (1965). J. Appl. Phys. 36. 20242031.CrossRefGoogle Scholar
de Wolf, P. M. and Sas, W. H. (1969). Acta Cryst. A25, 206209.CrossRefGoogle Scholar