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X-ray powder diffraction data for inclusion complex of β-cyclodextrin with fraxinellone

Published online by Cambridge University Press:  16 April 2013

Qing Wang ,
Li Li Zhang ,
Xiao Qing Wu ,
Qing Qing Pan ,
Yan Hong Su  and
Hui Li
Qing Wang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Li Li Zhang
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Xiao Qing Wu
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Qing Qing Pan
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Yan Hong Su
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
Hui Li*
Affiliation:
College of Chemical Engineering, Sichuan University, Chengdu 610065, China
*
a)Author to whom correspondence should be addressed. Electronic mail: lihuilab@sina.com
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Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for inclusion complex of β-cyclodextrin with fraxinellone, C42H70O35·C14H16O3·3H2O, are reported [a = 19.294(2) Å, b = 26.639(1) Å, c = 16.467(3) Å, β = 110.451(9)°, cell volume V = 7930.34 Å3, Z = 4 and space group C2]. All measured lines were indexed and are consistent with the C2 space group. No detectable impurities were observed.

Keywords

X-ray powder diffractionβ-cyclodextrinfraxinelloneinclusion complex
Type
New Diffraction Data
Information
Powder Diffraction , Volume 28 , Issue 3 , September 2013 , pp. 234 - 236
Copyright
Copyright © International Centre for Diffraction Data 2013 

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References

Engel, G. E., Wilke, S., König, O., Harris, K. D. M., and Leusen, F. J. J. (1999). “PowderSolve—a complete package for crystal structure solution from powder diffraction patterns,” J. Appl. Crystallogr. 32, 1169–1179.CrossRefGoogle Scholar
Guo, P., Su, Y. H., Chen, Q., Pan, Q. Q., and Li, H. (2011). “Crystal structure determination of the β-cyclodextrin-p-aminobenzoic acid inclusion complex from powder X-ray diffraction data,” Carbohydr. Res. 346, 986–990.CrossRefGoogle ScholarPubMed
Lü, M., Wu, W. J., and Liu, H. X. (2010). “Effects of fraxinellone on the midgut ultrastructural changes of Mythimna separata Walker,” Pesticide Biochem. Physiol. 98, 263–268.CrossRefGoogle Scholar
Neumann, M. (2003). “X-Cell: a novel indexing algorithm for routine tasks and difficult cases,” J. Appl. Crystallogr. 36, 356–365.CrossRefGoogle Scholar
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin: powder X-ray diffraction versus single-crystal X-ray diffraction,” Chin. Sci. Bull. 57, 3867–3871.CrossRefGoogle Scholar
Saenger, W. and Steiner, T. (1998). “Cyclodextrin inclusion complexes: host–guest interactions and hydrogen-bonding networks,” Acta Crystallogr. Sect. A. 54, 798–805.CrossRefGoogle Scholar
Trudeau, S. P. and Morken, J. P. (2005). “Short and efficient total synthesis of fraxinellone limonoids using the stereoselective Oshima–Utimoto reaction,” Org. Lett. 7, 5465–5468.CrossRefGoogle Scholar