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X-ray powder diffraction data for thiamphenicol, C12H15Cl2NO5S

  • Hong Qin Yang (a1), Qing Wang (a1), Pei Xiao Tang (a1), Bin Tang (a1), Ya Ping Li (a1) and Hui Li (a1)...


X-ray powder diffraction data, unit-cell parameters, and space group for thiamphenicol, C12H15Cl2NO5S, are reported [a = 17.346(3), b = 15.341(0), c = 5.790 (2) Å, α = β = γ = 90°, unit-cell volume V = 1540.8(3) Å3, Z = 4, and space group P212121]. All measured lines were indexed and are consistent with the P212121 space group. No detectable impurities were observed.


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Boultif, A. and LoueÈr, D. (1991). “Indexing of powder diffraction patterns for low-symmetry lattices by the successive dichotomy method,” J. Appl. Crystallogr. 24, 987993.
de Wolff, P. M. (1968). “A simplified criterion for the reliability of a powder pattern indexing,” J. Appl. Crystallogr. 1, 108113.
Ghosh, M., Basak, A. K., and Mazumdar, S. K. (1987). “Structure of Thiamphenicol, D-threo-2,2-Dichloro-N-﹛2-hydroxy-1-(hydroxymethyl)-2-[4-(methylsulfonyl) phenyl]ethyl﹜ acetamide,” Acta Crystallogr. C 43, 15521555.
Kowalski, P. (2007). “Capillary electrophoretic determination of thiamphenicol in turkeys serum and its pharmacokinetic application,” J. Pharm. Biomed. Anal. 43, 222227.
Ma, Ch., Chen, H., Sun, N., Ye, Y., and Chen, H. X. (2012). “Preparation of molecularly imprinted polymer monolith with an analogue of thiamphenicol and application to selective solid-phase microextraction,” Food Anal. Methods 5, 12671275.
LoueÈr, D. and LoueÈr, M. (1972). “Methode d'essais et erreurs pour l'indexation automatique des diagrammes de poudre,” J. Appl. Crystallogr. 5, 271275.
Pan, Q. Q., Guo, P., Duan, J., Cheng, Q., and Li, H. (2012). “Comparative crystal structure determination of griseofulvin,” Chin. Sci. Bull. 57, 38673871.
Shin, W. and Kim, S. (1983). “The crystal and molecular structure of thiamphenicol,” Bull. Korean Chem. Soc. 4, 7983.
Smith, G. S. and Snyder, R. L. (1979). “FN: a criterion for rating powder diffraction patterns and evaluating the reliability of powder indexing,” J. Appl. Crystallogr. 12, 6065.
Tang, P. X., Wu, X. Q., Zhang, L. L., Cheng, Q., and Li, H. (2013). “X-ray powder diffraction data for norethindrone,” Powder Diffr. (USA). 29, 4647.


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