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An irreversible disappearance of the mechanical loss peak of an yttria-doped silicon nitride

  • T. Akatsu (a1), Y. Kawakami (a1), Y. Tanabe (a1), E. Yasuda (a1), K. Yamada (a2) and N. Kamiya (a2)...

Abstract

The internal friction of a silicon nitride with a sintering aid of yttrium oxide was measured from room temperature to 1400 °C. A mechanical loss peak was typically observed at 1000 °C on heating the as-sintered specimen; however, it disappeared on cooling. Also, the peak was not observed upon heating a specimen that had been heated above 1400 °C. When we carried out thermal cycling, raising terminal temperatures from 1050 to 1400 °C, the integrated intensity of the peak gradually decreased due to the progressive crystallization of a grain-boundary amorphous phase.

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a) Address all correspondence to this author.e-mail: Takashi_Akatsu@msl.titech.ac.jp

References

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Journal of Materials Research
  • ISSN: 0884-2914
  • EISSN: 2044-5326
  • URL: /core/journals/journal-of-materials-research
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