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Controllable synthesis of palladium nanoparticles via a simple sonoelectrochemical method

Published online by Cambridge University Press:  31 January 2011

Xiao-Feng Qiu ,
Jin-Zhong Xu ,
Jian-Ming Zhu ,
Jun-Jie Zhu ,
Shu Xu  and
Hong-Yuan Chen
Xiao-Feng Qiu
Affiliation:
Laboratory of Mesoscopie Materials Science, Department of Chemistry, Nanjing University, Nanjing 210093, People's Republic of China
Jin-Zhong Xu
Affiliation:
Laboratory of Mesoscopie Materials Science, Department of Chemistry, Nanjing University, Nanjing 210093, People's Republic of China
Jian-Ming Zhu
Affiliation:
National Laboratory of Solid State Microstructures, Nanjing University, Nanjing, 210093, People's Republic of China
Jun-Jie Zhu*
Affiliation:
Laboratory of Mesoscopie Materials Science, Department of Chemistry, Nanjing University, Nanjing 210093, People's Republic of China
Shu Xu
Affiliation:
Laboratory of Mesoscopie Materials Science, Department of Chemistry, Nanjing University, Nanjing 210093, People's Republic of China
Hong-Yuan Chen
Affiliation:
Laboratory of Mesoscopie Materials Science, Department of Chemistry, Nanjing University, Nanjing 210093, People's Republic of China
*
a)Address all correspondence to this author. e-mail: jjzhu@nju.edu.cn
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Abstract

A simple pulse sonoelectrochemical technique was used to synthesize highly dispersed spherical palladium particles and a dendritic Pd superstructure in the presence of cethyltrimethylammonium bromide (CTAB) at room temperature. The shape and size of spherical nanocrystalline Pd can be controlled by varying current density, the interval between two continuous ultrasonic pulses, ultrasonic intensity, and the concentration of CTAB. The possible growth mechanism of dendritic-structured Pd is discussed.

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Type
Articles
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Journal of Materials Research , Volume 18 , Issue 6 , June 2003 , pp. 1399 - 1404
Copyright
Copyright © Materials Research Society 2003

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