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Study on the nature of the electrochemically synthesized hard Fe–15.4 mass% Ni–0.70 mass% C alloy film

Published online by Cambridge University Press:  06 January 2012

A. S. M. A. Haseeb ,
Y. Hayashi ,
M. Masuda  and
M. Arita
A. S. M. A. Haseeb
Affiliation:
Department of Materials and Metallurgical Engineering, Bangladesh University of Engineering and Technology (BUET), Dhaka 1000, Bangladesh
Y. Hayashi
Affiliation:
Department of Materials Science and Engineering, Kyushu University, 6–10–1 Hakozaki, Higashi-ku, Fukuoka 812–8581, Japan
M. Masuda
Affiliation:
Department of Materials Science and Engineering, Kyushu University, 6–10–1 Hakozaki, Higashi-ku, Fukuoka 812–8581, Japan
M. Arita
Affiliation:
Department of Materials Science and Engineering, Kyushu University, 6–10–1 Hakozaki, Higashi-ku, Fukuoka 812–8581, Japan
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Abstract

Electrochemical synthesis of hard Fe–15.4 mass% Ni–0.70 mass% C alloy film with a hardness 750 HV was carried out from sulfate-based bath containing a small amount of citric acid and L-ascorbic acid. The nature of the alloy was investigated by different characterization techniques including x-ray diffraction, x-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, Mössbauer spectroscopy, differential scanning calorimetry, and magnetic measurements. The decomposition behavior of the alloy was also studied and compared with that of thermally prepared martensite. It was found that the electrochemically deposited Fe–Ni–C alloy exists in a state that is ahead of the freshly quenched state of martensite. It is suggested that the state of the electrochemically deposited Fe–15.4 mass% Ni–0.70 mass% C alloy corresponds to the state of thermal martensite, which had been heated to the preprecipitation stage of tempering.

Type
Articles
Information
Journal of Materials Research , Volume 18 , Issue 4 , April 2003 , pp. 840 - 847
Copyright
Copyright © Materials Research Society 2003

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