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Cross dating (Th/U-14C) of calcite covering prehistoric paintings in Borneo

  • Valérie Plagnes (a1), Christiane Causse (a1), Michel Fontugne (a1), Hélène Valladas (a1), Jean-Michel Chazine (a2) and Luc-Henri Fage (a3)...

Abstract

We present the first application of cross-dating (Th/U measured by thermo-ionization mass spectrometry (TIMS) and 14C measured by accelerator mass spectrometry (AMS)) of calcite covering prehistoric paintings. Th/U age estimates of cave drapery range from 9800 to 27,300 yr B.P. while conventional 14C age is estimated between 9900 and 7610 yr B.P. depending on the dead carbon correction. The age discrepancy is attributed to a disturbance of Th/U and/or 14C geochemical systems, showing the limits of the geochronological approach applied to this kind of material. For the Th/U system, the poor consistency of U data (U content, 234U/238U activity ratios) and apparent ages argue for open system conditions. For 14C system, variation of the dead carbon fraction (dcf) and a possible mixing of successive generations of calcite could account for age discrepancy. Nevertheless, one sample shows concordant ages for the two methods. Compatible ages through corrections for open system conditions are assumed for other samples. Then, the cross-dating suggests 9900 yr as the minimum age of the piece of drapery; the underlying painting must be older. This study of rock art demonstrates the presence of a Pleistocene population before 9900 yr in the southeast of Borneo, whereas previously the only population in evidence in this area was of Austronesian type from ∼5000 to 6000 yrs ago.

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Beck, J.W., Richards, D.A., Edwards, R.L., Silverman, B.W., Smart, P.L., Donahue, D.J., Hererra-Osterheld, S., Burr, G.S., Calsoyas, L., Jull, A.J.T., and Biddulph, D., (2001). Extremely large variations of atmospheric 14C concentration during the last glacial period. Science 292, 2453 2458.
Bellwood, P., (1985). Prehistory of Indo-Malaysian Archipelago. Academic Press, Sydney.
Bellwood, P., Fox, J.J., Tryon, D., (1995). The Austronesians. Research School of Pacific studies, Canberra., pp. 96111.
Bischoff, J.L., Rosenbauer, R.J., Tavoso, A., Lumley, H., de, (1988). A test of uranium-series dating of fossil tooth enamel.: results from Tourmal Cave, France., Applied Geochemistry 3, 145151.
Bischoff, J.L., Ludwig, K., Garcia, J.F., Carbonell, E., Vaquero, M., Stafford, T.W., and Jull, A.J.T., (1994). Dating of the basal Aurignacian sandwich at Abric Romani (Catalunya, Spain) by radiocarbon and uranium-series. Journal of Archaeological Science 21, 541 551.
Causse, C., and Vincent, J.S., (1989). Th/U disequilibrium dating of middle and late Pleistocene wood and shelf from Banks and Victoria islands, Artic Canada. Canadian Journal of Earth Sciences 26, 2718 2723.
Chazine, J.M., (1995). Nouvelles perspectives archéologiques à Bornéo, Kalimantan. L’Anthropologie 99, 4 667 670.
Chazine, J.M., and Fage, L.H., (1998). La ligne de Wallace a-t-elle été franchie par les artistes des temps préhistoriques? Deux nouvelles grottes ornées à Bornéo (E Kalimantan). Karstologia 32, 39 46.
Chazine, J.M., and Fage, L.H., (1999). Préhistoire. découverte de grottes ornées à Bornéo. Archeologia 352, 12 19.
Clottes, J., Chauvet, J.M., Brunel-Deschamps, E., Hillaire, C., Daugas, J.P., Arnold, M., Cachier, H., Evin, J., Fortin, P., Oberlin, C., Tisnérat, N., and Valladas, H., (1995). Les peintures paléolithiques de la grotte Chauvet-Pont d’Arc, à Vallon-Pont-d’ Arc (Ardèche, France). datations directes et indirectes par la méthode du radiocarbone, C.R. Acad. Sci. Paris 320, 1133 1140.
Delagnes, A., Tournepiche, J.-F., Armand, D., Desclaux, E., Diot, M.-F., Ferrier, C., Le Fillâtre, V., and Vandermeersch, B., (1999). Le gisement Pléistocène moyen et supérieur d’Artenac (Saint-Mary, Charente). premier bilan interdisciplinaire. Bull. de la Société Préhistorique Française 96, 469 496.
Fage, L.H., Chazine, J.M., (2001). L’art pariétal des grottes de Kalimantan (Indonésie). Bilan de 10 années de prospection. Découvertes récentes de juin 2001 et perpectives de protection.; in: Actes du IIe Congrès national de Spéléologie, Genève., septembre 2001
Falguères, C., Lumley, H.de, and Bischoff, J.L., (1992). U-series dates on stalagmitic flowstone E (Riss/Würm interglacial) at grotte du Lazaret, Nice. Quaternary Research 38, 227 233.
Falguères, C., Bahain, J.J., and Saleki, H., (1997). U-series and ESR dating of teeth from Acheulian and Mousterian levels at La Micoque (Dordogne, France). Journal of Archaeological Science 24, 537 545.
Fontugne, M., Arnold, M., Labeyrie, L., Paterne, M., Calvert, S.E., and Duplessy, J.C. (1994). Palaeoenvironment, sapropel chronology and Nile River discharge during the last 20,000 years as indicated by deep sea sediment records in the eastern Mediterranean. in: Bar-Yosef, O., Kra, R.S. (Eds.), Late Quaternary Chronology and Paleoclimates of the Eastern Mediterranean, . Radiocarbon., pp. 7588.
Ford, D., and Williams, P., (1989). Karst Geomorphology and Hydrology. Unwin Hyman, London.
Gaven, C., (1975). Déséquilibre dans les familles radioactives de l’uranium et du Thorium au cours des processus volcano-génétiques. Thesis, Pierre et Marie Curie Univ, Paris.
Genty, D., Baker, A., Massault, M., Proctor, C., Gilmour, M., Pons-Branchu, E., and Hamelin, B., (2001). Dead carbon in stalagmites. carbonate bedrock paleodissolution vs. ageing of soil organic matter. Implications for 13C variations in speleothems. Geochimica Cosmochimica Acta 65, 3443 3457.
Genty, D., and Massault, M., (1997). Bomb 14C recorded in laminated speleothems. calculation of dead carbon proportion. Radiocarbon 39, 33 48.
Genty, D., Massault, M., Gilmour, M., Baker, A., Verheyden, S., and Kepens, E., (1999). Calculation of the past dead carbon proportion and variability by the comparison of AMS 14C and TIMS U/Th ages on two holocene stalagmites. Radiocarbon 41, 251 270.
Gill, J.B., Pyle, D.M., and Williams, R.W., (1992). Igneous rocks. Ivanovich, M., and Harmon, R.S. Uranium-Series Disequilibrium. Application to Earth, Marine and Environmental Sciences. second edition Oxford Science, New York. 207 258.
Grün, R., Schwarcz, H.P., and Chadam, J.M., (1988). ESR dating of tooth enamel. coupled correction for U-uptake and U-series disequilibrium. Nuclear Tracks and Radiation Measurements 14, 237 241.
Harrisson, T., (1957). The great cave of Niah. Man 57, 161 166.
Harrisson, T., (1972). The Borneo stone-age in the light of recent research. Sarawak Museum Journal VXX 40-41, 385 412.
McDermott, F., Grün, R., Stringer, C.B., and Hawkesworth, C.J., (1993). Mass-spectrometric U-series dates for Israeli Neanderthal/early modern hominid sites. Nature 363, 252 254.
Overpeck, J., Anderson, D., Trumbore, S., and Prell, W., (1996). The southwest Indian Monsoon over the last 18 000 years. Climate Dynamics 12, 213 225.
Plagnes, V., Causse, Ch., Genty, D., Paterne, M., and Blamart, D. (2002). A climatic record from 187 to 74 ka from a speleothem of the Clamouse Cave (South of France). Earth and Planetary Sciences Letters 201, 87103.
Reeder, R.J., Nugent, M., Tait, C.D., Morris, D.E., Heald, S.M., Beck, K.M., Hess, W.P., and Lanzirotti, A., (2001). Coprecipitation of Uranium (VI) with calcite. XAFS, micro-XAS, and luminescence characterization. Geochimica Cosmochimica Acta 65, 3491 3503.
Roberts, R.G., (1997). Luminescence dating in archaeology. Radiation Measurements 27, 819 892.
Roberts, R.G., Walsh, G., Murray, A., Olley, J., Jones, R., Morwood, M., Tuniz, C., Lawson, E., Macphail, M., Bowdery, D., and Naumann, I., (1997). Luminescence dating of rock art and past environments using mud-wasp nests in northern Australia. Nature 387, 696 699.
Rossignol-Strick, M., (1983). African monsoon, an immediate climate response to orbital insolation. Nature 304, 46 49.
Russ, J., Hyman, M., Shafer, H.J., and Rowe, M.W., (1990). Radiocarbon dating of prehistoric rock paintings by selective oxidation of organic carbon. Nature 348, 710 711.
Sirocko, F., Sarnthein, M., Erlenkeuser, H., Lange, H., Arnold, M., and Duplessy, J.C., (1993). Century-scale events in monsoonal climate over the past 24,000 years. Nature 364, 322 324.
Stuiver, M., Riemer, P.J., Bard, E., Beck, J.W., Burr, G.S., Hughen, K.A., Kromer, B., McCormac, G., Van Der Plicht, J., and Spurk, M., (1998). INTCAL 98 radiocarbon age calibration, 24,000-0 cal BP. Radiocarbon 40, 1041 1083.
Sturchio, N.C., Antonio, M.R., Soderholm, L., Sutton, S.R., and Brannon, J.C., (1998). Tetravalent uranium in calcite. Science 281, 971 973.
Tisnerat-Labordes, N., Poupeau, J.J., Tannau, J.F., Paterne, M., (2001). Development of an automated system for routine preparation of carbonate samples. Radiocarbon., in press
Turney, C.S.M., Bird, M.I., Fifield, L.K., Roberts, R.G., Smith, M., Dortch, C.E., Grün, R., Lawson, E., Ayliffe, L.K., Miller, G.H., Dortch, J., and Cresswell, R.G., (2001). Early human occupation at Devil’s Lair, Southwestern Australia 50,000 years ago. Quaternary Research 55, 3 13.
Valladas, H., Cachier, H., Arnold, M., and Lorblanchet, M., (1990). AMS C-14 dates for the prehistoric Cougnac Cave paintings, 5e Coll. Intern.. AMS (Poster), Paris.
Valladas, H., Cachier, H., Maurice, P., Bernardo de Quiros, F., Clottes, J., Cabrera Valdés, V., Uzquiamo, P., and Arnold, M., (1992). Direct radiocarbon dates for prehistoric paintings at the Altamira, El Castillo and Niaux caves. Nature 357, 68 70.
Wang, L., Sarnthein, M., Erlenkeuser, H., Grimalt, J., Grootes, P., Heilig, S., Ivanova, E., Kienast, M., Pelejero, C., and Pflaumann, U., (1999). East Asian monsoon climate during the Late Pleitocene. high resolution sediment records from the South China Sea. Marine Geology 156, 245 284.

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